6-phenyl-4H-<1,2,4>triazolo<4,3-a><1,4>benzodiazepin-4-ylamine formate salt

Base Information

Chemical Name:6-phenyl-4H-<1,2,4>triazolo<4,3-a><1,4>benzodiazepin-4-ylamine formate salt
CAS No.:111113-18-9
Molecular Formula:CH₂O₂*C₁₆H₁₃N₅
Molecular Weight:321.338
Hs Code.:

Synonyms:6-phenyl-4H-<1,2,4>triazolo<4,3-a><1,4>benzodiazepin-4-ylamine formate salt

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Chemical Property of 6-phenyl-4H-<1,2,4>triazolo<4,3-a><1,4>benzodiazepin-4-ylamine formate salt

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Technology Process of 6-phenyl-4H-<1,2,4>triazolo<4,3-a><1,4>benzodiazepin-4-ylamine formate salt

There total 5 articles about 6-phenyl-4H-<1,2,4>triazolo<4,3-a><1,4>benzodiazepin-4-ylamine formate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 64-18-6
formic acid

: 111113-15-6
6-Phenyl-4-benzyloxycarbonylamino-4H-[1,2,4]triazolo-[4,3-a][1,4]benzodiazepine

: 111113-18-9
6-phenyl-4H-<1,2,4>triazolo<4,3-a><1,4>benzodiazepin-4-ylamine formate salt

Guidance literature:: palladium on activated charcoal; In methanol; water; for 1.5h;
DOI:10.1021/jm00396a028

Reference yield:

: 111113-15-6
6-Phenyl-4-benzyloxycarbonylamino-4H-[1,2,4]triazolo-[4,3-a][1,4]benzodiazepine

: 111113-18-9
6-phenyl-4H-<1,2,4>triazolo<4,3-a><1,4>benzodiazepin-4-ylamine formate salt

Guidance literature:: With formic acid; palladium; In methanol;

Reference yield:

: 108895-98-3
benzyl 2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-ylcarbamate

: 111113-18-9
6-phenyl-4H-<1,2,4>triazolo<4,3-a><1,4>benzodiazepin-4-ylamine formate salt

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / Lawesson's reagent / toluene / 5 h / 110 °C

2: NH₂NH₂ / methanol / 1.5 h / 23 °C

3: 65 percent / H₂SO₄ / ethanol / 10 h / 23 °C

4: 90 percent / Pd/C / methanol; H₂O / 1.5 h

With Lawessons reagent; sulfuric acid; hydrazine; palladium on activated charcoal; In methanol; ethanol; water; toluene;
DOI:10.1021/jm00396a028