trans-dicarbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P)ruthenium(II)

Base Information

Chemical Name:trans-dicarbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P)ruthenium(II)
CAS No.:109063-35-6
Molecular Formula:C₃₂H₃₄Cl₂O₄P₂Ru
Molecular Weight:716.543
Hs Code.:

Synonyms:trans-dicarbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P)ruthenium(II)

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Chemical Property of trans-dicarbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P)ruthenium(II)

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Technology Process of trans-dicarbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P)ruthenium(II)

There total 2 articles about trans-dicarbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 109011-63-4
trans-dichloro-cis-bis((2-methoxyethyl)diphenylphosphane-O,P)ruthenium(II) * ethanol

: 109063-35-6
trans-dicarbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P)ruthenium(II)

Guidance literature:: With CO; In dichloromethane; CO is introduced to a soln. of Ru-compd. at 0°C for 30 min (Ar or N2).; Pptn. with CO-saturated n-hexane, recrystn. from CH2Cl2/n-hexane under CO below 20°C and dried at 20°C under flowing CO, elem. anal.;

Reference yield: 82.0%

: 109011-71-4
cis-dicarbonyl-cis-dichloro-trans-bis((2-methoxyethyl)diphenylphosphane-P)ruthenium(II)

: 109063-35-6
trans-dicarbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P)ruthenium(II)

Guidance literature:: With CO; In tetrahydrofuran; Irradiation (UV/VIS); Irradiation at -20°C for 1 h under CO.; Pptn. with CO saturated n-hexane, elem. anal.;

Reference yield: 82.0%

: 109011-62-3
trans-dichlorobis((2-methoxyethyl)diphenylphosphine-O,P)ruthenium(II)

: 109063-35-6
trans-dicarbonyl-trans-dichloro-trans-bis((2-methoxyethyl)diphenyl phosphane-P)ruthenium(II)

: 109011-66-7
Cl₂Ru(CO)((C₆H₅)2PCH₂CH₂OCH₃)2

Guidance literature:: In dichloromethane; Ar atmosphere; stirring (30 min, room temp.); partial evapn. (vac.), pptn. on addn. of hexane, filtration, washing (hexane), drying (vac.); elem. anal.;