[1-phosphono-3-[4-[[2-(tritylthio)ethyl][[2-(tritylthio)ethylcarbamoyl]methyl]amino]butyrylamino]propyl]phosphonic acid tetraethyl ester

Base Information

Chemical Name:[1-phosphono-3-[4-[[2-(tritylthio)ethyl][[2-(tritylthio)ethylcarbamoyl]methyl]amino]butyrylamino]propyl]phosphonic acid tetraethyl ester
CAS No.:848087-35-4
Molecular Formula:C₅₉H₇₃N₃O₈P₂S₂
Molecular Weight:1078.32
Hs Code.:

Synonyms:[1-phosphono-3-[4-[[2-(tritylthio)ethyl][[2-(tritylthio)ethylcarbamoyl]methyl]amino]butyrylamino]propyl]phosphonic acid tetraethyl ester

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Chemical Property of [1-phosphono-3-[4-[[2-(tritylthio)ethyl][[2-(tritylthio)ethylcarbamoyl]methyl]amino]butyrylamino]propyl]phosphonic acid tetraethyl ester

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Technology Process of [1-phosphono-3-[4-[[2-(tritylthio)ethyl][[2-(tritylthio)ethylcarbamoyl]methyl]amino]butyrylamino]propyl]phosphonic acid tetraethyl ester

There total 4 articles about [1-phosphono-3-[4-[[2-(tritylthio)ethyl][[2-(tritylthio)ethylcarbamoyl]methyl]amino]butyrylamino]propyl]phosphonic acid tetraethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.3%

: 141473-49-6
tetraethyl 3-aminopropylidene-1,1-bisphosphonate

: 228253-41-6
N-[2-(tritylthio)ethylaminocarbonylmethyl]-N-[2-(tritylthio)ethyl]-4-aminobutyric acid

: 848087-35-4
[1-phosphono-3-[4-[[2-(tritylthio)ethyl][[2-(tritylthio)ethylcarbamoyl]methyl]amino]butyrylamino]propyl]phosphonic acid tetraethyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In chloroform; at 20 ℃; for 5h;
DOI:10.1002/jlcr.864

Reference yield:

: 136496-87-2
tetraethyl 3-nitropropylidene-1,1-bisphosphonate

: 848087-35-4
[1-phosphono-3-[4-[[2-(tritylthio)ethyl][[2-(tritylthio)ethylcarbamoyl]methyl]amino]butyrylamino]propyl]phosphonic acid tetraethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol; H₂O / 6 h / 20 °C

2: 65.3 percent / DCC / CHCl₃ / 5 h / 20 °C

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; chloroform; water;
DOI:10.1002/jlcr.864

Reference yield:

: 152863-83-7
N-[2-[(triphenylmethyl)thio]ethyl]-2-[[2-[(triphenylmethyl)thio]ethyl]amino]acetamide

: 848087-35-4
[1-phosphono-3-[4-[[2-(tritylthio)ethyl][[2-(tritylthio)ethylcarbamoyl]methyl]amino]butyrylamino]propyl]phosphonic acid tetraethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 52.9 percent / ethyldiisopropylamine / dimethylformamide / 3 h / 90 °C

2: 98 percent / NaOH

3: 65.3 percent / DCC / CHCl₃ / 5 h / 20 °C

With sodium hydroxide; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In chloroform; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.864