N-[2-(tritylthio)ethylaminocarbonylmethyl]-N-[2-(tritylthio)ethyl]-4-aminobutyric acid

Base Information

Chemical Name:N-[2-(tritylthio)ethylaminocarbonylmethyl]-N-[2-(tritylthio)ethyl]-4-aminobutyric acid
CAS No.:228253-41-6
Molecular Formula:C₄₈H₄₈N₂O₃S₂
Molecular Weight:765.053
Hs Code.:

Synonyms:N-[2-(tritylthio)ethylaminocarbonylmethyl]-N-[2-(tritylthio)ethyl]-4-aminobutyric acid

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Chemical Property of N-[2-(tritylthio)ethylaminocarbonylmethyl]-N-[2-(tritylthio)ethyl]-4-aminobutyric acid

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Technology Process of N-[2-(tritylthio)ethylaminocarbonylmethyl]-N-[2-(tritylthio)ethyl]-4-aminobutyric acid

There total 6 articles about N-[2-(tritylthio)ethylaminocarbonylmethyl]-N-[2-(tritylthio)ethyl]-4-aminobutyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 848087-34-3
4-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-butyric acid ethyl ester

: 228253-41-6
N-[2-(tritylthio)ethylaminocarbonylmethyl]-N-[2-(tritylthio)ethyl]-4-aminobutyric acid

Guidance literature:: With sodium hydroxide;
DOI:10.1002/jlcr.864

Reference yield: 95.0%

: 915380-02-8
4-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-butyric acid methyl ester

: 228253-41-6
N-[2-(tritylthio)ethylaminocarbonylmethyl]-N-[2-(tritylthio)ethyl]-4-aminobutyric acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2006.08.050

Reference yield:

: 152863-83-7
N-[2-[(triphenylmethyl)thio]ethyl]-2-[[2-[(triphenylmethyl)thio]ethyl]amino]acetamide

: 228253-41-6
N-[2-(tritylthio)ethylaminocarbonylmethyl]-N-[2-(tritylthio)ethyl]-4-aminobutyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / KI; K₂CO₃ / acetonitrile

2: 95 percent / aq. NaOH / tetrahydrofuran

With sodium hydroxide; potassium carbonate; potassium iodide; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.bmcl.2006.08.050