((CH₃)3C₆H₂)2Ge(OCH₃)CHCl₂

Base Information

• Chemical Name: ((CH₃)3C₆H₂)2Ge(OCH₃)CHCl₂
• CAS No.: 956146-20-6
• Molecular Formula: C₂₀H₂₆Cl₂GeO
• Molecular Weight: 425.922
• Mol file: 956146-20-6.mol

Synonyms:((CH₃)3C₆H₂)2Ge(OCH₃)CHCl₂

Chemical Property of ((CH₃)3C₆H₂)2Ge(OCH₃)CHCl₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ((CH₃)3C₆H₂)2Ge(OCH₃)CHCl₂

There total 2 articles about ((CH₃)3C₆H₂)2Ge(OCH₃)CHCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

methanol (67-56-1) + dimesitylfluoro(trichloro)germane (956146-17-1) → ((CH3)3C6H2)2Ge(OCH3)CHCl2 (956146-20-6)

Guidance literature:

With t-BuLi; In tetrahydrofuran; methanol; hexane; (Ar); std. Schlenk technique; soln. of BuLi in hexane was added to soln.of Ge compd. in THF at -110°C; stirred at -80°C for 30 mi n; MeOH was added; slowly warmed to room temp. within 2 h; filtered; concd. (vac.); cooled in pentane at -20°C;

DOI:10.1021/om061188j

Reference yield:

dimesityldifluorogermane (96481-36-6) → ((CH3)3C6H2)2Ge(OCH3)CHCl2 (956146-20-6)

Guidance literature:

Multi-step reaction with 2 steps

1: n-BuLi / tetrahydrofuran; chloroform; hexane

2: t-BuLi / tetrahydrofuran; methanol; hexane

With n-BuLi; t-BuLi; In tetrahydrofuran; methanol; hexane; chloroform;

DOI:10.1021/om061188j

upstream raw materials:

methanol

dimesitylfluoro(trichloro)germane

dimesityldifluorogermane