[3,5-dibromo-4-(3-formyl-4-methoxy-phenoxy)-phenyl]-acetic acid methyl ester

Base Information

Chemical Name:[3,5-dibromo-4-(3-formyl-4-methoxy-phenoxy)-phenyl]-acetic acid methyl ester
CAS No.:725239-16-7
Molecular Formula:C₁₇H₁₄Br₂O₅
Molecular Weight:458.103
Hs Code.:

Synonyms:[3,5-dibromo-4-(3-formyl-4-methoxy-phenoxy)-phenyl]-acetic acid methyl ester

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Chemical Property of [3,5-dibromo-4-(3-formyl-4-methoxy-phenoxy)-phenyl]-acetic acid methyl ester

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Technology Process of [3,5-dibromo-4-(3-formyl-4-methoxy-phenoxy)-phenyl]-acetic acid methyl ester

There total 5 articles about [3,5-dibromo-4-(3-formyl-4-methoxy-phenoxy)-phenyl]-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 4885-02-3
Dichloromethyl methyl ether

: 348167-06-6
3,5-Dibromo-4-(4-methoxyphenoxy)phenylacetic acid methyl ester

: 725239-16-7
[3,5-dibromo-4-(3-formyl-4-methoxy-phenoxy)-phenyl]-acetic acid methyl ester

Guidance literature:: Dichloromethyl methyl ether; 3,5-Dibromo-4-(4-methoxyphenoxy)phenylacetic acid methyl ester; tin(IV) chloride; In dichloromethane; at -60 - 0 ℃; for 6h; Inert atmosphere;

With hydrogenchloride; In dichloromethane; water; for 0.333333h;

Reference yield:

: 100-66-3
methoxybenzene

: 725239-16-7
[3,5-dibromo-4-(3-formyl-4-methoxy-phenoxy)-phenyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: I₂; HNO₃; Ac₂O / TFA

1.2: aq. NaBF₄

2.1: Cu; Et₃N / CH₂Cl₂

3.1: SnCl₄ / CH₂Cl₂ / 0 °C

With iodine; nitric acid; acetic anhydride; tin(IV) chloride; copper; triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2004.04.032

Reference yield:

: 14199-15-6
Methyl 4-hydroxyphenylacetate

: 725239-16-7
[3,5-dibromo-4-(3-formyl-4-methoxy-phenoxy)-phenyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: aq. Br₂ / 20 °C

2: Cu; Et₃N / CH₂Cl₂

3: SnCl₄ / CH₂Cl₂ / 0 °C

With bromine; tin(IV) chloride; copper; triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2004.04.032