(4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)fluoroacetic acid ethyl ester

Base Information

Chemical Name:(4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)fluoroacetic acid ethyl ester
CAS No.:1186634-15-0
Molecular Formula:C₃₄H₃₅FN₂O₄S
Molecular Weight:586.727
Hs Code.:

Synonyms:(4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)fluoroacetic acid ethyl ester

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Chemical Property of (4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)fluoroacetic acid ethyl ester

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Technology Process of (4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)fluoroacetic acid ethyl ester

There total 10 articles about (4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)fluoroacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1186634-26-3
4-(4-cyclohexylbenzyloxy)benzaldehyde

: 1186634-14-9
fluoro(4-(3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)acetic acid ethyl ester

: 1186634-15-0
(4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)fluoroacetic acid ethyl ester

Guidance literature:: With piperidine; In ethanol; for 20h; Reflux;

Reference yield:

: 121986-07-0,137766-69-9,13312-80-6
p-nitromandelonitrile

: 1186634-15-0
(4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)fluoroacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride / water; acetic acid / 4 h / 100 °C

1.2: 4 h / 80 - 85 °C

2.1: hydrogen / palladium on activated charcoal / methanol / 4 h

3.1: ethanol / 6 h / Reflux

4.1: triethylamine / ethanol / 5 h / Reflux

5.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / 10 °C / Inert atmosphere

6.1: piperidine / ethanol / 20 h / Reflux

With piperidine; hydrogenchloride; diethylamino-sulfur trifluoride; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; acetic acid;

Reference yield:

4-nitro-mandelic acid-ethyl ester: 13312-87-3
4-nitro-mandelic acid-ethyl ester

: 1186634-15-0
(4-(5-(1-(4-(4-cyclohexylbenzyloxy)phenyl)methylidene)-3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)fluoroacetic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen / palladium on activated charcoal / methanol / 4 h

2: ethanol / 6 h / Reflux

3: triethylamine / ethanol / 5 h / Reflux

4: diethylamino-sulfur trifluoride / dichloromethane / 1 h / 10 °C / Inert atmosphere

5: piperidine / ethanol / 20 h / Reflux

With piperidine; diethylamino-sulfur trifluoride; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane;