fluoro(4-(3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)acetic acid ethyl ester

Base Information

Chemical Name:fluoro(4-(3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)acetic acid ethyl ester
CAS No.:1186634-14-9
Molecular Formula:C₁₄H₁₅FN₂O₃S
Molecular Weight:310.349
Hs Code.:

Synonyms:fluoro(4-(3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)acetic acid ethyl ester

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Chemical Property of fluoro(4-(3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)acetic acid ethyl ester

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Technology Process of fluoro(4-(3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)acetic acid ethyl ester

There total 6 articles about fluoro(4-(3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.5%

: 1186634-12-7
hydroxy(4-(3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)acetic acid ethyl ester

: 1186634-14-9
fluoro(4-(3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)acetic acid ethyl ester

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at 10 ℃; for 1h; Inert atmosphere;

Reference yield:

: 121986-07-0,137766-69-9,13312-80-6
p-nitromandelonitrile

: 1186634-14-9
fluoro(4-(3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride / water; acetic acid / 4 h / 100 °C

1.2: 4 h / 80 - 85 °C

2.1: hydrogen / palladium on activated charcoal / methanol / 4 h

3.1: ethanol / 6 h / Reflux

4.1: triethylamine / ethanol / 5 h / Reflux

5.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / 10 °C / Inert atmosphere

With hydrogenchloride; diethylamino-sulfur trifluoride; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; acetic acid;

Reference yield:

4-nitro-mandelic acid-ethyl ester: 13312-87-3
4-nitro-mandelic acid-ethyl ester

: 1186634-14-9
fluoro(4-(3-methyl-4-oxothiazolidin-2-ylideneamino)phenyl)acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / palladium on activated charcoal / methanol / 4 h

2: ethanol / 6 h / Reflux

3: triethylamine / ethanol / 5 h / Reflux

4: diethylamino-sulfur trifluoride / dichloromethane / 1 h / 10 °C / Inert atmosphere

With diethylamino-sulfur trifluoride; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane;