4-chlorophenyl piperidine-1-carbodithioate

Base Information

Chemical Name:4-chlorophenyl piperidine-1-carbodithioate
CAS No.:16913-56-7
Molecular Formula:C₁₂H₁₄ClNS₂
Molecular Weight:271.835
Hs Code.:

Synonyms:4-chlorophenyl piperidine-1-carbodithioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chlorophenyl piperidine-1-carbodithioate

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Technology Process of 4-chlorophenyl piperidine-1-carbodithioate

There total 3 articles about 4-chlorophenyl piperidine-1-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 110-89-4
piperidine

: 75-15-0,12122-00-8
carbon disulfide

: 637-87-6
1-Chloro-4-iodobenzene

: 16913-56-7
4-chlorophenyl piperidine-1-carbodithioate

Guidance literature:: piperidine; carbon disulfide; In neat (no solvent); for 0.166667h; Cooling; Green chemistry;

1-Chloro-4-iodobenzene; With CuO-Fe₃O₄; In neat (no solvent); at 130 ℃; for 10h; Green chemistry;
DOI:10.1039/c5ra20524g

Reference yield: 63.0%

: 34220-01-4
di-(4-chlorophenyl)iodonium chloride

: 873-57-4
sodium piperidinedithiocarbamate

: 16913-56-7
4-chlorophenyl piperidine-1-carbodithioate

Guidance literature:: In acetonitrile; at 70 ℃; for 13h;
DOI:10.1021/jo00227a032

Reference yield:

: 110-89-4
piperidine

: 75-15-0,12122-00-8
carbon disulfide

: 4-chloro-2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 3-chlorophenyl piperidine-1-carbodithioate

: 16913-56-7
4-chlorophenyl piperidine-1-carbodithioate

Guidance literature:: piperidine; carbon disulfide; With potassium fluoride; 18-crown-6 ether; In tetrahydrofuran; for 0.0333333h; Sealed tube; Inert atmosphere;

4-chloro-2-(trimethylsilyl)phenyl trifluoromethanesulfonate; In tetrahydrofuran; at 25 ℃; for 12h; Overall yield = 73 percent; Overall yield = 0.05 g; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.1c03378