4'-(benzyloxy)-2'-(methoxymethoxy)-2-nitro-1,2,3,6-tetrahydro-1,1'-biphenyl

Base Information

Chemical Name:4'-(benzyloxy)-2'-(methoxymethoxy)-2-nitro-1,2,3,6-tetrahydro-1,1'-biphenyl
CAS No.:1382722-63-5
Molecular Formula:C₂₁H₂₃NO₅
Molecular Weight:369.417
Hs Code.:

Synonyms:4'-(benzyloxy)-2'-(methoxymethoxy)-2-nitro-1,2,3,6-tetrahydro-1,1'-biphenyl

Suppliers and Price of 4'-(benzyloxy)-2'-(methoxymethoxy)-2-nitro-1,2,3,6-tetrahydro-1,1'-biphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4'-(benzyloxy)-2'-(methoxymethoxy)-2-nitro-1,2,3,6-tetrahydro-1,1'-biphenyl

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4'-(benzyloxy)-2'-(methoxymethoxy)-2-nitro-1,2,3,6-tetrahydro-1,1'-biphenyl

There total 5 articles about 4'-(benzyloxy)-2'-(methoxymethoxy)-2-nitro-1,2,3,6-tetrahydro-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1382722-62-4
(Z)-4-(benzyloxy)-2-(methoxymethoxy)-1-(2-nitrovinyl)benzene

: 106-99-0,130983-70-9,29406-96-0,9003-17-2
buta-1,3-diene

: 1382722-63-5
4'-(benzyloxy)-2'-(methoxymethoxy)-2-nitro-1,2,3,6-tetrahydro-1,1'-biphenyl

Guidance literature:: In toluene; at -78 ℃; for 48h; Sealed tube; Reflux;

Reference yield:

: 52085-14-0
4-benzoxy-salicylaldehyde

: 1382722-63-5
4'-(benzyloxy)-2'-(methoxymethoxy)-2-nitro-1,2,3,6-tetrahydro-1,1'-biphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: ammonium acetate / 0.33 h / 50 °C

3: toluene / 48 h / -78 - 120 °C / Sealed tube

With ammonium acetate; N-ethyl-N,N-diisopropylamine; In dichloromethane; toluene; 2: Henry reaction;
DOI:10.1021/jm300544c

Reference yield:

: 95-01-2
2,4-Dihydroxybenzaldehyde

: 1382722-63-5
4'-(benzyloxy)-2'-(methoxymethoxy)-2-nitro-1,2,3,6-tetrahydro-1,1'-biphenyl

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / acetonitrile / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

3: ammonium acetate / 0.33 h / 50 °C

4: toluene / 48 h / -78 - 120 °C / Sealed tube

With ammonium acetate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; toluene; acetonitrile; 3: Henry reaction;
DOI:10.1021/jm300544c