(2S,3R)-2-hydroxy-3-(phenylsulfanyl)heptanoic acid (tetrahydropyran-2-yloxy)amide

Base Information

Chemical Name:(2S,3R)-2-hydroxy-3-(phenylsulfanyl)heptanoic acid (tetrahydropyran-2-yloxy)amide
CAS No.:285572-43-2
Molecular Formula:C₁₈H₂₇NO₄S
Molecular Weight:353.483
Hs Code.:

Synonyms:(2S,3R)-2-hydroxy-3-(phenylsulfanyl)heptanoic acid (tetrahydropyran-2-yloxy)amide

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Chemical Property of (2S,3R)-2-hydroxy-3-(phenylsulfanyl)heptanoic acid (tetrahydropyran-2-yloxy)amide

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Technology Process of (2S,3R)-2-hydroxy-3-(phenylsulfanyl)heptanoic acid (tetrahydropyran-2-yloxy)amide

There total 3 articles about (2S,3R)-2-hydroxy-3-(phenylsulfanyl)heptanoic acid (tetrahydropyran-2-yloxy)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 6723-30-4
O-2-tetrahydro-2H-pyranhydroxylamine

: 285572-42-1
(2S,3R)-2-hydroxy-3-(phenylsulfanyl)heptanoic acid

: 285572-43-2
(2S,3R)-2-hydroxy-3-(phenylsulfanyl)heptanoic acid (tetrahydropyran-2-yloxy)amide

Guidance literature:: With benzotriazol-1-ol; 1,1'-carbonyldiimidazole; In acetonitrile; Heating;
DOI:10.1021/jm000018k

Reference yield:

: 132665-45-3,181378-55-2
(2R,3S)-3-butyloxirane-2-carboxylic acid

: 285572-43-2
(2S,3R)-2-hydroxy-3-(phenylsulfanyl)heptanoic acid (tetrahydropyran-2-yloxy)amide

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / LiClO₄; Al₂O₃ / CH₂Cl₂ / 20 °C

2: 18 percent / 1,1'-hydroybenzotriazole; 1,1'-carbonyldiimidazole / acetonitrile / Heating

With aluminum oxide; lithium perchlorate; benzotriazol-1-ol; 1,1'-carbonyldiimidazole; In dichloromethane; acetonitrile; 1: Addition / 2: Condensation;
DOI:10.1021/jm000018k

Reference yield:

: 97275-47-3
(2S,3S)-(3-butyloxiranyl)methyl alcohol

: 285572-43-2
(2S,3R)-2-hydroxy-3-(phenylsulfanyl)heptanoic acid (tetrahydropyran-2-yloxy)amide

Guidance literature:: Multi-step reaction with 3 steps

1: 28 percent / RuO₂; NaIO₄ / CH₂Cl₂; acetonitrile; H₂O / 24 h / pH 4.5

2: 28 percent / LiClO₄; Al₂O₃ / CH₂Cl₂ / 20 °C

3: 18 percent / 1,1'-hydroybenzotriazole; 1,1'-carbonyldiimidazole / acetonitrile / Heating

With ruthenium(IV) oxide; aluminum oxide; sodium periodate; lithium perchlorate; benzotriazol-1-ol; 1,1'-carbonyldiimidazole; In dichloromethane; water; acetonitrile; 1: Oxidation / 2: Addition / 3: Condensation;
DOI:10.1021/jm000018k