(2S,3R)-3-benzenesulfinyl-2-hydroxyheptanoic acid (tetrahydropyran-2-yloxy)amide

Base Information

Chemical Name:(2S,3R)-3-benzenesulfinyl-2-hydroxyheptanoic acid (tetrahydropyran-2-yloxy)amide
CAS No.:285572-44-3
Molecular Formula:C₁₈H₂₇NO₅S
Molecular Weight:369.482
Hs Code.:

Synonyms:(2S,3R)-3-benzenesulfinyl-2-hydroxyheptanoic acid (tetrahydropyran-2-yloxy)amide

Suppliers and Price of (2S,3R)-3-benzenesulfinyl-2-hydroxyheptanoic acid (tetrahydropyran-2-yloxy)amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,3R)-3-benzenesulfinyl-2-hydroxyheptanoic acid (tetrahydropyran-2-yloxy)amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,3R)-3-benzenesulfinyl-2-hydroxyheptanoic acid (tetrahydropyran-2-yloxy)amide

There total 5 articles about (2S,3R)-3-benzenesulfinyl-2-hydroxyheptanoic acid (tetrahydropyran-2-yloxy)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 285572-43-2
(2S,3R)-2-hydroxy-3-(phenylsulfanyl)heptanoic acid (tetrahydropyran-2-yloxy)amide

: 285572-44-3
(2S,3R)-3-benzenesulfinyl-2-hydroxyheptanoic acid (tetrahydropyran-2-yloxy)amide

Guidance literature:: With N-(benzenesulfonyl)-3-phenyloxaziridine; In dichloromethane; at 20 ℃;
DOI:10.1021/jm000018k

Reference yield:

: 6723-30-4
O-2-tetrahydro-2H-pyranhydroxylamine

: 285572-44-3
(2S,3R)-3-benzenesulfinyl-2-hydroxyheptanoic acid (tetrahydropyran-2-yloxy)amide

Guidance literature:: Multi-step reaction with 2 steps

1: 18 percent / 1,1'-hydroybenzotriazole; 1,1'-carbonyldiimidazole / acetonitrile / Heating

2: 52 percent / 3-phenyl-2-(phenylsulfonyl)oxaziridine / CH₂Cl₂ / 20 °C

With benzotriazol-1-ol; N-(benzenesulfonyl)-3-phenyloxaziridine; 1,1'-carbonyldiimidazole; In dichloromethane; acetonitrile; 1: Condensation / 2: Oxidation;
DOI:10.1021/jm000018k

Reference yield:

: 132665-45-3,181378-55-2
(2R,3S)-3-butyloxirane-2-carboxylic acid

: 285572-44-3
(2S,3R)-3-benzenesulfinyl-2-hydroxyheptanoic acid (tetrahydropyran-2-yloxy)amide

Guidance literature:: Multi-step reaction with 3 steps

1: 28 percent / LiClO₄; Al₂O₃ / CH₂Cl₂ / 20 °C

2: 18 percent / 1,1'-hydroybenzotriazole; 1,1'-carbonyldiimidazole / acetonitrile / Heating

3: 52 percent / 3-phenyl-2-(phenylsulfonyl)oxaziridine / CH₂Cl₂ / 20 °C

With aluminum oxide; lithium perchlorate; benzotriazol-1-ol; N-(benzenesulfonyl)-3-phenyloxaziridine; 1,1'-carbonyldiimidazole; In dichloromethane; acetonitrile; 1: Addition / 2: Condensation / 3: Oxidation;
DOI:10.1021/jm000018k