S,S-diphenyl N²-isobutyryl-5'-O-dimethoxytritylguanosine 3'-phosphorodithioate

Base Information

Chemical Name:S,S-diphenyl N²-isobutyryl-5'-O-dimethoxytritylguanosine 3'-phosphorodithioate
CAS No.:85571-16-0
Molecular Formula:C₄₇H₄₆N₅O₈PS₂
Molecular Weight:904.017
Hs Code.:

S,S-diphenyl N<sup>2</sup>-isobutyryl-5'-O-dimethoxytritylguanosine 3'-phosphorodithioate

Synonyms:S,S-diphenyl N²-isobutyryl-5'-O-dimethoxytritylguanosine 3'-phosphorodithioate

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Chemical Property of S,S-diphenyl N²-isobutyryl-5'-O-dimethoxytritylguanosine 3'-phosphorodithioate

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Technology Process of S,S-diphenyl N²-isobutyryl-5'-O-dimethoxytritylguanosine 3'-phosphorodithioate

There total 5 articles about S,S-diphenyl N²-isobutyryl-5'-O-dimethoxytritylguanosine 3'-phosphorodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 67941-87-1
cyclohexylammonium S,S-diphenyl phosphorodithioate

: 93966-65-5
5'-O-(bis(4-methoxyphenyl)phenylmethyl)-2'-deoxy-N-(2-methyl-1-oxopropyl)guanosine 3'-benzoate

: 85571-16-0
S,S-diphenyl N²-isobutyryl-5'-O-dimethoxytritylguanosine 3'-phosphorodithioate

Guidance literature:: With dapsone; In pyridine; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(01)87448-2

Reference yield: 60.0%

: 67941-87-1
cyclohexylammonium S,S-diphenyl phosphorodithioate

: 68892-41-1
5'-O-dimethoxytrityl-N-isobutyryldeoxyguanosine

: 85571-16-0
S,S-diphenyl N²-isobutyryl-5'-O-dimethoxytritylguanosine 3'-phosphorodithioate

: 103655-43-2
Dithiophosphoric acid O-{9-[(2R,4S,5R)-5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(bis-phenylsulfanyl-phosphoryloxy)-tetrahydro-furan-2-yl]-2-isobutyrylamino-9H-purin-6-yl} ester S,S'-diphenyl ester

Guidance literature:: With 4,6-dimethoxybenzene-1,3-bis(sulfonyl) chloride; In pyridine; for 29h; Product distribution; other amount of reagents, and reaction times;
DOI:10.1016/S0040-4020(01)96778-X

Reference yield:

: 68892-41-1
5'-O-dimethoxytrityl-N-isobutyryldeoxyguanosine

: 85571-16-0
S,S-diphenyl N²-isobutyryl-5'-O-dimethoxytritylguanosine 3'-phosphorodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / pyridine / 2 h / Ambient temperature

2: 81 percent / DDS / pyridine / 2 h / Ambient temperature

With dapsone; In pyridine;
DOI:10.1016/S0040-4020(01)87448-2