Technology Process of (R)-benzyl (2-(tert-butylsulfinyl)-6-(methoxymethoxy)phenyl) sulfane
There total 3 articles about (R)-benzyl (2-(tert-butylsulfinyl)-6-(methoxymethoxy)phenyl) sulfane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C12H18O3S2;
With
sodium hydroxide;
In
ethanol;
at 20 ℃;
for 0.333333h;
Inert atmosphere;
benzyl bromide;
In
ethanol;
at 20 ℃;
Inert atmosphere;
DOI:10.1016/j.tetasy.2011.02.031
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrahydrofuran / 1 h / -78 - -50 °C / basic condition; Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: sodium hydroxide / ethanol / 0.33 h / 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
With
sodium hydroxide;
In
tetrahydrofuran; ethanol;
DOI:10.1016/j.tetasy.2011.02.031
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: tetrahydrofuran / 1 h / -78 - -50 °C / basic condition; Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: sodium hydroxide / ethanol / 0.33 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
With
n-butyllithium; sodium hydroxide;
In
tetrahydrofuran; ethanol;
DOI:10.1016/j.tetasy.2011.02.031
