N-(4'-Methoxy[1,1'-biphenyl]-2-yl)benzamide

Base Information

Chemical Name:N-(4'-Methoxy[1,1'-biphenyl]-2-yl)benzamide
CAS No.:54147-92-1
Molecular Formula:C₂₀H₁₇NO₂
Molecular Weight:303.36
Hs Code.:
DSSTox Substance ID:DTXSID601261045

Synonyms:N-(4'-Methoxy[1,1'-biphenyl]-2-yl)benzamide;DTXSID601261045;54147-92-1

Suppliers and Price of N-(4'-Methoxy[1,1'-biphenyl]-2-yl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4'-Methoxy[1,1'-biphenyl]-2-yl)benzamide

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:303.125928785
Heavy Atom Count:23
Complexity:370

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2=CC=CC=C2NC(=O)C3=CC=CC=C3

Technology Process of N-(4'-Methoxy[1,1'-biphenyl]-2-yl)benzamide

There total 8 articles about N-(4'-Methoxy[1,1'-biphenyl]-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 38089-03-1
2-(4-methoxyphenyl)aniline

: 98-88-4
benzoyl chloride

: 54147-92-1
N-(4'-methoxy-biphenyl-2-yl)-benzamide

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1055/s-0030-1258081

Reference yield: 85.0%

: 15310-02-8
o-iodobenzanilide

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 54147-92-1
N-(4'-methoxy-biphenyl-2-yl)-benzamide

Guidance literature:: 4-methoxyphenyl magnesium bromide; With CuCN*2LiCl; In tetrahydrofuran; 1,2-dimethoxyethane; for 0.333333h;

o-iodobenzanilide; iron(III)-acetylacetonate; In tetrahydrofuran; 1,2-dimethoxyethane; at 80 ℃; for 4h; Further stages.;
DOI:10.1039/b618617c

Reference yield:

: 615-43-0
2-iodophenylamine

: 54147-92-1
N-(4'-methoxy-biphenyl-2-yl)-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 77 percent / AgCN / CH₂Cl₂; acetonitrile / 12 h / 20 °C

2.1: CuCN*2LiCl / tetrahydrofuran; 1,2-dimethoxy-ethane / 0.33 h

2.2: 85 percent / Fe(acac)3 / tetrahydrofuran; 1,2-dimethoxy-ethane / 4 h / 80 °C

With silver cyanide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; acetonitrile;
DOI:10.1039/b618617c