Technology Process of C19H32O4
There total 4 articles about C19H32O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium cerium (IV) nitrate; water;
In
acetonitrile;
at 20 ℃;
for 6h;
DOI:10.1021/ol901765f
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Jones reagent / acetone
2.1: sulfuric acid / 12 h / Reflux
3.1: iodine; magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux
3.2: 5 h / Inert atmosphere; Reflux
4.1: ammonium cerium (IV) nitrate / water; acetonitrile / 6 h / Cooling with ice
With
Jones reagent; ammonium cerium (IV) nitrate; sulfuric acid; iodine; magnesium;
In
diethyl ether; water; acetone; acetonitrile;
1.1: Jones oxidation;
DOI:10.1002/asia.201100480
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: iodine; magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux
1.2: 5 h / Inert atmosphere; Reflux
2.1: ammonium cerium (IV) nitrate / water; acetonitrile / 6 h / Cooling with ice
With
ammonium cerium (IV) nitrate; iodine; magnesium;
In
diethyl ether; water; acetonitrile;
DOI:10.1002/asia.201100480