2-methylallyl N-(perfluorobenzoyl)oxybenzimidothioate

Base Information

Chemical Name:2-methylallyl N-(perfluorobenzoyl)oxybenzimidothioate
CAS No.:1568950-27-5
Molecular Formula:C₁₈H₁₂F₅NO₂S
Molecular Weight:401.357
Hs Code.:

Synonyms:2-methylallyl N-(perfluorobenzoyl)oxybenzimidothioate

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Chemical Property of 2-methylallyl N-(perfluorobenzoyl)oxybenzimidothioate

Chemical Property:

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Technology Process of 2-methylallyl N-(perfluorobenzoyl)oxybenzimidothioate

There total 4 articles about 2-methylallyl N-(perfluorobenzoyl)oxybenzimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

pentafluorobenzoylchloride: 2251-50-5
pentafluorobenzoylchloride

: 15177-34-1
thiobenzhydroxamic acid

: 563-47-3
3-Chloro-2-methylpropene

: 1568950-27-5
2-methylallyl N-(perfluorobenzoyl)oxybenzimidothioate

Guidance literature:: thiobenzhydroxamic acid; 3-Chloro-2-methylpropene; With tetra-(n-butyl)ammonium iodide; triethylamine; In tetrahydrofuran; at 60 ℃;

pentafluorobenzoylchloride; With triethylamine; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1021/jo500080x

Reference yield:

: 100-52-7
benzaldehyde

: 1568950-27-5
2-methylallyl N-(perfluorobenzoyl)oxybenzimidothioate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine hydrochloride; sodium hydroxide / N,N-dimethyl-formamide; water / 1 h / 30 °C

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.1: sodium sulfide; triethylamine / diethyl ether; water / 1 h / 20 °C

4.1: triethylamine; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 60 °C

4.2: 0.5 h / 20 °C

With sodium sulfide; N-chloro-succinimide; hydroxylamine hydrochloride; tetra-(n-butyl)ammonium iodide; triethylamine; sodium hydroxide; In tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/jo500080x

Reference yield:

: 932-90-1
Benzaldoxime

: 1568950-27-5
2-methylallyl N-(perfluorobenzoyl)oxybenzimidothioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.1: sodium sulfide; triethylamine / diethyl ether; water / 1 h / 20 °C

3.1: triethylamine; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 60 °C

3.2: 0.5 h / 20 °C

With sodium sulfide; N-chloro-succinimide; tetra-(n-butyl)ammonium iodide; triethylamine; In tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/jo500080x