5-(4-Chlorphenyl)-2,2,2-trimethoxy-3,3-bis(trifluormethyl)-2,2-dihydro-1,4,2-oxazaphosphol-4-en

Base Information

• Chemical Name: 5-(4-Chlorphenyl)-2,2,2-trimethoxy-3,3-bis(trifluormethyl)-2,2-dihydro-1,4,2-oxazaphosphol-4-en
• CAS No.: 40683-75-8
• Molecular Formula: C₁₃H₁₃ClF₆NO₄P
• Molecular Weight: 427.668

Synonyms:5-(4-Chlorphenyl)-2,2,2-trimethoxy-3,3-bis(trifluormethyl)-2,2-dihydro-1,4,2-oxazaphosphol-4-en

Chemical Property of 5-(4-Chlorphenyl)-2,2,2-trimethoxy-3,3-bis(trifluormethyl)-2,2-dihydro-1,4,2-oxazaphosphol-4-en

Chemical Property:

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Technology Process of 5-(4-Chlorphenyl)-2,2,2-trimethoxy-3,3-bis(trifluormethyl)-2,2-dihydro-1,4,2-oxazaphosphol-4-en

There total 1 articles about 5-(4-Chlorphenyl)-2,2,2-trimethoxy-3,3-bis(trifluormethyl)-2,2-dihydro-1,4,2-oxazaphosphol-4-en which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-N-(2,2,2-trifluoro-1-trifluoromethyl-ethylidene)-benzamide (52786-52-4) + phosphorous acid trimethyl ester (121-45-9) → 5-(4-Chlorphenyl)-2,2,2-trimethoxy-3,3-bis(trifluormethyl)-2,2-dihydro-1,4,2-oxazaphosphol-4-en (40683-75-8)

Guidance literature:

In hexane;

Reference yield: 50.0%

isoquinoline (119-65-3) + 5-(4-Chlorphenyl)-2,2,2-trimethoxy-3,3-bis(trifluormethyl)-2,2-dihydro-1,4,2-oxazaphosphol-4-en (40683-75-8) → 3-(4-chloro-phenyl)-1,1-bis-trifluoromethyl-1,10b-dihydro-imidazo[5,1-a]isoquinoline (59118-74-0)

Guidance literature:

at 110 ℃; for 24h;

Reference yield: 39.0%

1,4-pyrazine (290-37-9) + 5-(4-Chlorphenyl)-2,2,2-trimethoxy-3,3-bis(trifluormethyl)-2,2-dihydro-1,4,2-oxazaphosphol-4-en (40683-75-8) → 3,8-Bis-(4-chloro-phenyl)-1,1,10,10-tetrakis-trifluoromethyl-1,10,10a,10b-tetrahydro-diimidazo[1,5-a;5',1'-c]pyrazine (78817-13-7)

Guidance literature:

In toluene; for 24h; Heating;

upstream raw materials:

4-chloro-N-(2,2,2-trifluoro-1-trifluoromethyl-ethylidene)-benzamide

phosphorous acid trimethyl ester

Downstream raw materials:

N-<2,2,2-Trifluor-1-(trifluormethyl)aethyl>-p-chlor-benzamid

3-(4-chloro-phenyl)-1,1-bis-trifluoromethyl-1,8a-dihydro-imidazo[1,5-a]pyridine

3,8-Bis-(4-chloro-phenyl)-1,1,10,10-tetrakis-trifluoromethyl-1,10,10a,10b-tetrahydro-diimidazo[1,5-a;5',1'-c]pyrazine

3-(4-chloro-phenyl)-1,1-bis-trifluoromethyl-1,10b-dihydro-imidazo[5,1-a]isoquinoline

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