C₃₀H₅₂O₅Si₂

Base Information

Chemical Name:C₃₀H₅₂O₅Si₂
CAS No.:1612781-09-5
Molecular Formula:C₃₀H₅₂O₅Si₂
Molecular Weight:548.911
Hs Code.:

C<sub>30</sub>H<sub>52</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₃₀H₅₂O₅Si₂

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Chemical Property of C₃₀H₅₂O₅Si₂

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Technology Process of C₃₀H₅₂O₅Si₂

There total 7 articles about C₃₀H₅₂O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 75-77-4
chloro-trimethyl-silane

: 1612781-03-9
C₂₇H₄₄O₅Si

: 1612781-09-5
C₃₀H₅₂O₅Si₂

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/anie.201310164

Reference yield:

: 89043-32-3
(4-bromobutoxy)-tert-butyldimethylsilane

: 1612781-09-5
C₃₀H₅₂O₅Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: magnesium; iodine / ethylene dibromide; tetrahydrofuran / 3 h / Reflux; Inert atmosphere

1.2: 2.5 h / -78 - 0 °C / Inert atmosphere

2.1: n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; lithium hexamethyldisilazane / hexane; tetrahydrofuran / 1 h / -78 - 0 °C / Inert atmosphere

2.2: 3.5 h / -78 - -30 °C / Inert atmosphere

3.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 3 h / 50 °C / Inert atmosphere

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2 h / 0 - 20 °C / pH 7 / Inert atmosphere

5.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.75 h / 0 - 20 °C / Inert atmosphere

6.1: calcium hydride; dicyclohexylboron chloride; triethylamine / benzene; diethyl ether / 1.08 h / -78 - 0 °C / Inert atmosphere

6.2: 17.5 h / -78 - -20 °C / Inert atmosphere

7.1: 1H-imidazole / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; calcium hydride; dicyclohexylboron chloride; iodine; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; magnesium; triethylamine; 1,1,1,3,3,3-hexamethyl-disilazane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane; dichloromethane; ethylene dibromide; benzene; 3.1: |Suzuki Coupling;
DOI:10.1002/anie.201310164

Reference yield:

: 1612780-81-0
C₂₂H₃₈O₄Si

: 1612781-09-5
C₃₀H₅₂O₅Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; lithium hexamethyldisilazane / hexane; tetrahydrofuran / 1 h / -78 - 0 °C / Inert atmosphere

1.2: 3.5 h / -78 - -30 °C / Inert atmosphere

2.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 3 h / 50 °C / Inert atmosphere

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 2 h / 0 - 20 °C / pH 7 / Inert atmosphere

4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.75 h / 0 - 20 °C / Inert atmosphere

5.1: calcium hydride; dicyclohexylboron chloride; triethylamine / benzene; diethyl ether / 1.08 h / -78 - 0 °C / Inert atmosphere

5.2: 17.5 h / -78 - -20 °C / Inert atmosphere

6.1: 1H-imidazole / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; calcium hydride; dicyclohexylboron chloride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; triethylamine; 1,1,1,3,3,3-hexamethyl-disilazane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane; dichloromethane; benzene; 2.1: |Suzuki Coupling;
DOI:10.1002/anie.201310164