(2R)-toluene-4-sulfonic acid 2-hydroxynonyl ester

Base Information

Chemical Name:(2R)-toluene-4-sulfonic acid 2-hydroxynonyl ester
CAS No.:208589-17-7
Molecular Formula:C₁₆H₂₆O₄S
Molecular Weight:314.446
Hs Code.:

Synonyms:(2R)-toluene-4-sulfonic acid 2-hydroxynonyl ester

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Chemical Property of (2R)-toluene-4-sulfonic acid 2-hydroxynonyl ester

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Technology Process of (2R)-toluene-4-sulfonic acid 2-hydroxynonyl ester

There total 5 articles about (2R)-toluene-4-sulfonic acid 2-hydroxynonyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 98-59-9
p-toluenesulfonyl chloride

: 118969-84-9
(R)-Nonane-1,2-diol

: 208589-17-7
(2R)-toluene-4-sulfonic acid 2-hydroxynonyl ester

Guidance literature:: With dmap; di(n-butyl)tin oxide; triethylamine; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1002/cjoc.201500315

Reference yield: 45.0%

: C₁₈H₂₈O₅S

: C₁₈H₂₈O₅S

: C₁₈H₂₈O₅S

: 208589-17-7
(2R)-toluene-4-sulfonic acid 2-hydroxynonyl ester

Guidance literature:: lipase PS (Burkholderia cepacia); In phosphate buffer; di-isopropyl ether; at 30 ℃; for 24h;
DOI:10.1055/s-2008-1032047

Reference yield:

: 3761-92-0
n-hexylmagnesium bromide

: 113826-06-5,6746-81-2
(R)-glycidyl tosylate

: 208589-17-7
(2R)-toluene-4-sulfonic acid 2-hydroxynonyl ester

Guidance literature:: With dilithium tetrachlorocuprate; Yield given. Multistep reaction; 1.) THF, ether, -35 deg C, 40 min, 2.) THF, ether, ether, 3 h;
DOI:10.1021/jm980162u