ethyl 2-(4-octylphenoxy)acetate

Base Information

Chemical Name:ethyl 2-(4-octylphenoxy)acetate
CAS No.:1621517-92-7
Molecular Formula:C₁₈H₂₈O₃
Molecular Weight:292.419
Hs Code.:

Synonyms:ethyl 2-(4-octylphenoxy)acetate

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Chemical Property of ethyl 2-(4-octylphenoxy)acetate

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Technology Process of ethyl 2-(4-octylphenoxy)acetate

There total 1 articles about ethyl 2-(4-octylphenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1806-26-4
p-Octylphenol

: 105-36-2
ethyl bromoacetate

: 1621517-92-7
ethyl 2-(4-octylphenoxy)acetate

Guidance literature:: With potassium carbonate; In acetone; for 5h; Reflux;

Reference yield: 82.0%

: 1621517-92-7
ethyl 2-(4-octylphenoxy)acetate

: 51437-89-9
2-(4-octylphenoxy)ethanol

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; hexane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jm500192s

Reference yield:

: 1621517-92-7
ethyl 2-(4-octylphenoxy)acetate

: 1621517-48-3
2-(4-octylphenoxy)-1-(thiazol-2-yl)ethanone

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / diethyl ether; hexane / 2 h / 0 - 20 °C / Inert atmosphere

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite; sodium bromide; sodium hydrogencarbonate / water; ethyl acetate; toluene / 1 h / 0 °C

3.1: n-butyllithium / diethyl ether; hexane / 0.17 h / -78 °C / Inert atmosphere

3.2: 2.5 h / -78 - 20 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

With sodium hypochlorite; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; sodium bromide; In diethyl ether; hexane; dichloromethane; water; ethyl acetate; toluene; 4.1: |Dess-Martin Oxidation;
DOI:10.1021/jm500192s