C₃₀H₂₃BrO₂S

Base Information

Chemical Name:C₃₀H₂₃BrO₂S
CAS No.:1312997-41-3
Molecular Formula:C₃₀H₂₃BrO₂S
Molecular Weight:527.481
Hs Code.:

C<sub>30</sub>H<sub>23</sub>BrO<sub>2</sub>S

Synonyms:C₃₀H₂₃BrO₂S

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Chemical Property of C₃₀H₂₃BrO₂S

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Technology Process of C₃₀H₂₃BrO₂S

There total 3 articles about C₃₀H₂₃BrO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 62784-66-1
bis(1-naphthyl)methanol

: 18739-77-0
2-<(4-bromophenyl)thio>propionic acid

: 1312997-41-3
C₃₀H₂₃BrO₂S

Guidance literature:: 2-<(4-bromophenyl)thio>propionic acid; With benzoic acid anhydride; N-ethyl-N,N-diisopropylamine; In ⁽²⁾H₈-toluene; at 20 ℃; for 0.0833333h; Resolution of racemate;

bis(1-naphthyl)methanol; With 2-phenyl-3,4-dihydro-2H-benzo[4,5]thiazolo[3,2-a]pyrimidine; In ⁽²⁾H₈-toluene; at 20 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Resolution of racemate;
DOI:10.1002/anie.201007860

Reference yield:

: 1213744-28-5
(S)-di-(1-naphthyl)methyl α-(phenylthio)propanoate

: 1312997-41-3
C₃₀H₂₃BrO₂S

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h

2.1: benzoic acid anhydride; N-ethyl-N,N-diisopropylamine / ⁽²⁾H₈-toluene / 0.08 h / 20 °C / Resolution of racemate

2.2: 24 h / 20 °C / Resolution of racemate

With lithium aluminium tetrahydride; benzoic acid anhydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ⁽²⁾H₈-toluene;
DOI:10.1002/anie.201007860

Reference yield:

: 106-53-6
para-bromobenzenethiol

: 1312997-41-3
C₃₀H₂₃BrO₂S

Guidance literature:: Multi-step reaction with 2 steps

1.1: Basic conditions

2.1: benzoic acid anhydride; N-ethyl-N,N-diisopropylamine / ⁽²⁾H₈-toluene / 0.08 h / 20 °C / Resolution of racemate

2.2: 24 h / 20 °C / Resolution of racemate

With benzoic acid anhydride; N-ethyl-N,N-diisopropylamine; In ⁽²⁾H₈-toluene;
DOI:10.1002/anie.201007860