Methyl 2-(tert-butoxycarbonylamino)-3-(3,4-dichlorobenzylamino) propionate

Base Information

Chemical Name:Methyl 2-(tert-butoxycarbonylamino)-3-(3,4-dichlorobenzylamino) propionate
CAS No.:178261-23-9
Molecular Formula:C₁₆H₂₂Cl₂N₂O₄
Molecular Weight:377.268
Hs Code.:

Synonyms:Methyl 2-(tert-butoxycarbonylamino)-3-(3,4-dichlorobenzylamino) propionate

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Chemical Property of Methyl 2-(tert-butoxycarbonylamino)-3-(3,4-dichlorobenzylamino) propionate

Chemical Property:

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Technology Process of Methyl 2-(tert-butoxycarbonylamino)-3-(3,4-dichlorobenzylamino) propionate

There total 3 articles about Methyl 2-(tert-butoxycarbonylamino)-3-(3,4-dichlorobenzylamino) propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 55477-80-0
methyl 2-[(tert-butoxycarbonyl)amino]acrylate

: 102-49-8
3,4-dichlorobenzyl amine

: 178261-23-9
Methyl 2-(tert-butoxycarbonylamino)-3-(3,4-dichlorobenzylamino) propionate

Guidance literature:: In methanol;
DOI:10.1016/S0960-894X(98)00320-5

Reference yield:

: 69942-12-7
N-tert-butoxycarbonylserine methyl ester

: 178261-23-9
Methyl 2-(tert-butoxycarbonylamino)-3-(3,4-dichlorobenzylamino) propionate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂

2: Et₂NH / diethyl ether; ethyl acetate

3: 41 percent / methanol

With pyridine; diethylamine; In methanol; diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1016/S0960-894X(98)00320-5

Reference yield:

: 69961-11-1
2-tert-butoxycarbonylamino-3-(toluene-4-sulfonyloxy)-propionic acid methyl ester

: 178261-23-9
Methyl 2-(tert-butoxycarbonylamino)-3-(3,4-dichlorobenzylamino) propionate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₂NH / diethyl ether; ethyl acetate

2: 41 percent / methanol

With diethylamine; In methanol; diethyl ether; ethyl acetate;
DOI:10.1016/S0960-894X(98)00320-5