Methyl 2-(tert-butoxycarbonylamino)-3-(N-methyl-3,4-dichlorobenzylamino)propionate

Base Information

Chemical Name:Methyl 2-(tert-butoxycarbonylamino)-3-(N-methyl-3,4-dichlorobenzylamino)propionate
CAS No.:178261-28-4
Molecular Formula:C₁₇H₂₄Cl₂N₂O₄
Molecular Weight:391.295
Hs Code.:

Synonyms:Methyl 2-(tert-butoxycarbonylamino)-3-(N-methyl-3,4-dichlorobenzylamino)propionate

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Chemical Property of Methyl 2-(tert-butoxycarbonylamino)-3-(N-methyl-3,4-dichlorobenzylamino)propionate

Chemical Property:

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Technology Process of Methyl 2-(tert-butoxycarbonylamino)-3-(N-methyl-3,4-dichlorobenzylamino)propionate

There total 6 articles about Methyl 2-(tert-butoxycarbonylamino)-3-(N-methyl-3,4-dichlorobenzylamino)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 144-55-8
sodium hydrogencarbonate

: 178261-23-9
Methyl 2-(tert-butoxycarbonylamino)-3-(3,4-dichlorobenzylamino) propionate

: 178261-28-4
Methyl 2-(tert-butoxycarbonylamino)-3-(N-methyl-3,4-dichlorobenzylamino)propionate

Guidance literature:: With formaldehyd; sodium cyanoborohydride; acetic acid; In acetonitrile;

Reference yield:

: 69942-12-7
N-tert-butoxycarbonylserine methyl ester

: 178261-28-4
Methyl 2-(tert-butoxycarbonylamino)-3-(N-methyl-3,4-dichlorobenzylamino)propionate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / CH₂Cl₂

2: Et₂NH / diethyl ether; ethyl acetate

3: 41 percent / methanol

4: NaCNBH₃, AcOH / acetonitrile

With pyridine; sodium cyanoborohydride; acetic acid; diethylamine; In methanol; diethyl ether; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/S0960-894X(98)00320-5

Reference yield:

: 55477-80-0
methyl 2-[(tert-butoxycarbonyl)amino]acrylate

: 178261-28-4
Methyl 2-(tert-butoxycarbonylamino)-3-(N-methyl-3,4-dichlorobenzylamino)propionate

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / methanol

2: NaCNBH₃, AcOH / acetonitrile

With sodium cyanoborohydride; acetic acid; In methanol; acetonitrile;
DOI:10.1016/S0960-894X(98)00320-5