4-methoxy-3'-(2''-nitrobenzene-α-azoxy)-4'-hydroxyazobenzene

Base Information

• Chemical Name: 4-methoxy-3'-(2''-nitrobenzene-α-azoxy)-4'-hydroxyazobenzene
• CAS No.: 120124-71-2
• Molecular Formula: C₁₉H₁₅N₅O₅
• Molecular Weight: 393.359
• Mol file: 120124-71-2.mol

Synonyms:4-methoxy-3'-(2''-nitrobenzene-α-azoxy)-4'-hydroxyazobenzene

Chemical Property of 4-methoxy-3'-(2''-nitrobenzene-α-azoxy)-4'-hydroxyazobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-methoxy-3'-(2''-nitrobenzene-α-azoxy)-4'-hydroxyazobenzene

There total 1 articles about 4-methoxy-3'-(2''-nitrobenzene-α-azoxy)-4'-hydroxyazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

4-methoxybenzenediazonium tetrafluoroborate (459-64-3) + potassium salt of the o-dinitrobenzene anion radical → methoxybenzene (100-66-3) + 4-methoxy-3'-(2''-nitrobenzene-α-azoxy)-4'-hydroxyazobenzene (120124-71-2) + 1,2-Dinitrobenzene (528-29-0)

Guidance literature:

In tetrahydrofuran; at -30 ℃; for 1h; Product distribution; also in DMSO and in the presence of 18-crown-6;

DOI:10.1007/BF00961116

upstream raw materials:

4-methoxybenzenediazonium tetrafluoroborate