mer-hydrido[[(methoxycarbonyl)methyl]cyano](methyl cyanoacetate)tris (triphenylphosphine)ruthenium(II)

Base Information

Chemical Name:mer-hydrido[[(methoxycarbonyl)methyl]cyano](methyl cyanoacetate)tris (triphenylphosphine)ruthenium(II)
CAS No.:138614-12-7
Molecular Formula:C₆₂H₅₅N₂O₄P₃Ru
Molecular Weight:1086.12
Hs Code.:

Synonyms:mer-hydrido[[(methoxycarbonyl)methyl]cyano](methyl cyanoacetate)tris (triphenylphosphine)ruthenium(II)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of mer-hydrido[[(methoxycarbonyl)methyl]cyano](methyl cyanoacetate)tris (triphenylphosphine)ruthenium(II)

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Technology Process of mer-hydrido[[(methoxycarbonyl)methyl]cyano](methyl cyanoacetate)tris (triphenylphosphine)ruthenium(II)

There total 1 articles about mer-hydrido[[(methoxycarbonyl)methyl]cyano](methyl cyanoacetate)tris (triphenylphosphine)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 27599-25-3,54083-06-6,19529-00-1
dihydridotetrakis(triphenylphosphine)ruthenium

: 105-34-0
methyl 2-cyanoacetate

: 138614-12-7
mer-hydrido[[(methoxycarbonyl)methyl]cyano](methyl cyanoacetate)tris (triphenylphosphine)ruthenium(II)

Guidance literature:: In tetrahydrofuran; byproducts: H2; room temp., 7 h;
DOI:10.1021/ja00155a008

Reference yield: 94.0%

: 138614-12-7
mer-hydrido[[(methoxycarbonyl)methyl]cyano](methyl cyanoacetate)tris (triphenylphosphine)ruthenium(II)

: 201230-82-2
carbon monoxide

: 173828-21-2,173594-00-8
hydrido[[(methoxycarbonyl)methyl]cyano]dicarbonylbis(triphenylphosphine)ruthenium(II)

Guidance literature:: In benzene-d6; byproducts: methyl cyanoacetate; 1 h;
DOI:10.1021/ja00155a008

Reference yield: 60.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 138614-12-7
mer-hydrido[[(methoxycarbonyl)methyl]cyano](methyl cyanoacetate)tris (triphenylphosphine)ruthenium(II)

: Ru₂Cl₄(NCCH₂COOCH₃)(P(C₆H₅)3)4*C₄H₈O

Guidance literature:: In tetrahydrofuran; byproducts: H2, methyl cyanoacetate; stirring (room temp., 19 h), removal (vac.); recrystn. (THF/hexane);
DOI:10.1021/ja00155a008