ATB-429

Base Information

Chemical Name:ATB-429
CAS No.:947152-51-4
Molecular Formula:C₂₁H₁₉NO₅S₃
Molecular Weight:461.584
Hs Code.:

Synonyms:ATB-429

Suppliers and Price of ATB-429

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ATB-429

Chemical Property:

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Technology Process of ATB-429

There total 4 articles about ATB-429 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.8%

: 18274-81-2
desmethyl anethole trithione

: 135321-95-8
2-hydroxy-5-<(tert-butoxycarbonyl)amino>benzoic acid

: 947152-51-4
ATB-429

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 8h; Inert atmosphere;
DOI:10.1016/j.bmcl.2016.03.012

Reference yield:

: 18274-81-2
desmethyl anethole trithione

: 947152-51-4
ATB-429

Guidance literature:: 2-hydroxy-5-<(tert-butoxycarbonyl)amino>benzoic acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

desmethyl anethole trithione; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 75h;

Reference yield:

: 532-11-6
anethole trithione

: 947152-51-4
ATB-429

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine hydrochloride / 2 h / 215 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 8 h / 0 - 20 °C / Inert atmosphere

With dmap; pyridine hydrochloride; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.bmcl.2016.03.012