tert-butyldimethylsilyl 2-{5-nitro-2-[(E)-2-phenylethenyl]-1H-imidazol-1-yl}ethyl ether

Base Information

Chemical Name:tert-butyldimethylsilyl 2-{5-nitro-2-[(E)-2-phenylethenyl]-1H-imidazol-1-yl}ethyl ether
CAS No.:304015-71-2
Molecular Formula:C₁₉H₂₇N₃O₃Si
Molecular Weight:373.527
Hs Code.:

Synonyms:tert-butyldimethylsilyl 2-{5-nitro-2-[(E)-2-phenylethenyl]-1H-imidazol-1-yl}ethyl ether

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Chemical Property of tert-butyldimethylsilyl 2-{5-nitro-2-[(E)-2-phenylethenyl]-1H-imidazol-1-yl}ethyl ether

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Technology Process of tert-butyldimethylsilyl 2-{5-nitro-2-[(E)-2-phenylethenyl]-1H-imidazol-1-yl}ethyl ether

There total 3 articles about tert-butyldimethylsilyl 2-{5-nitro-2-[(E)-2-phenylethenyl]-1H-imidazol-1-yl}ethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 38318-92-2
2-{5-nitro-2-[(E)-2-phenylethenyl]-1H-imidazol-1-yl}ethanol

: 69739-34-0
t-butyldimethylsiyl triflate

: 304015-71-2
tert-butyldimethylsilyl 2-{5-nitro-2-[(E)-2-phenylethenyl]-1H-imidazol-1-yl}ethyl ether

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/jm030308b

Reference yield:

: 100-52-7
benzaldehyde

: 304015-71-2
tert-butyldimethylsilyl 2-{5-nitro-2-[(E)-2-phenylethenyl]-1H-imidazol-1-yl}ethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 26 percent / Na; DMSO; MeOH / 24 h / 20 °C

2: 100 percent / pyridine / CH₂Cl₂ / 16 h / 20 °C

With pyridine; methanol; sodium; dimethyl sulfoxide; In dichloromethane;
DOI:10.1021/jm030308b

Reference yield:

: 443-48-1
metronidazole

: 304015-71-2
tert-butyldimethylsilyl 2-{5-nitro-2-[(E)-2-phenylethenyl]-1H-imidazol-1-yl}ethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 26 percent / Na; DMSO; MeOH / 24 h / 20 °C

2: 100 percent / pyridine / CH₂Cl₂ / 16 h / 20 °C

With pyridine; methanol; sodium; dimethyl sulfoxide; In dichloromethane;
DOI:10.1021/jm030308b