4-(4-(1-((4-azidobutananoyl)oxy)ethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

Base Information

Chemical Name:4-(4-(1-((4-azidobutananoyl)oxy)ethyl)-2-methoxy-5-nitrophenoxy)butanoic acid
CAS No.:1351396-38-7
Molecular Formula:C₁₇H₂₂N₄O₈
Molecular Weight:410.384
Hs Code.:

Synonyms:4-(4-(1-((4-azidobutananoyl)oxy)ethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

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Chemical Property of 4-(4-(1-((4-azidobutananoyl)oxy)ethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

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Technology Process of 4-(4-(1-((4-azidobutananoyl)oxy)ethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

There total 5 articles about 4-(4-(1-((4-azidobutananoyl)oxy)ethyl)-2-methoxy-5-nitrophenoxy)butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 947386-28-9
4-azidobutanoic acid anhydride

: 175281-76-2
4-[4-(1-hydroxyethyl)-2-methoxy-5-nitrophenoxy]butanoic acid

: 1351396-38-7
4-(4-(1-((4-azidobutananoyl)oxy)ethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

Guidance literature:: In dichloromethane;
DOI:10.1002/anie.201106463

Reference yield:

: 1031702-80-3
ethyl 4-(4-acetyl-2-methoxy-5-nitrophenoxy)butanoate

: 1351396-38-7
4-(4-(1-((4-azidobutananoyl)oxy)ethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate; ethanol / 38 °C / Inert atmosphere

2: trifluoroacetic acid; water / 30 h / 90 °C / Inert atmosphere

3: dmap; pyridine / dichloromethane / 20 °C / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; ethanol; water; trifluoroacetic acid; In dichloromethane;

Reference yield:

: 498-02-2
1-(3-methoxy-4-hydroxyphenyl)ethanone

: 1351396-38-7
4-(4-(1-((4-azidobutananoyl)oxy)ethyl)-2-methoxy-5-nitrophenoxy)butanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: nitric acid / 0.01 h / Cooling with ice; Inert atmosphere

3: sodium tetrahydroborate; ethanol / 38 °C / Inert atmosphere

4: trifluoroacetic acid; water / 30 h / 90 °C / Inert atmosphere

5: dmap; pyridine / dichloromethane / 20 °C / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; ethanol; water; nitric acid; potassium carbonate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;