C₁₇H₂₈OSSi

Base Information

Chemical Name:C₁₇H₂₈OSSi
CAS No.:1547458-57-0
Molecular Formula:C₁₇H₂₈OSSi
Molecular Weight:308.56
Hs Code.:

Synonyms:C₁₇H₂₈OSSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₂₈OSSi

Chemical Property:

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Technology Process of C₁₇H₂₈OSSi

There total 1 articles about C₁₇H₂₈OSSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 70-11-1
α-bromoacetophenone

: 156275-96-6
triisopropylsilanethiol

: 1547458-57-0
C₁₇H₂₈OSSi

Guidance literature:: triisopropylsilanethiol; With triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

α-bromoacetophenone; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol403709g

Reference yield: 93.0%

: 1547458-57-0
C₁₇H₂₈OSSi

: 74-88-4
methyl iodide

: 1547458-69-4
C₁₈H₃₀OSSi

Guidance literature:: C₁₇H₂₈OSSi; With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane; In tetrahydrofuran; at -78 - 0 ℃; for 2.5h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol403709g

Reference yield: 86.0%

: 1547458-57-0
C₁₇H₂₈OSSi

: 220913-60-0
(3-bromoprop-1-yn-1-yl)triethylsilane

: 1547458-73-0
C₂₆H₄₄OSSi₂

Guidance literature:: C₁₇H₂₈OSSi; With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane; In tetrahydrofuran; at -78 - 0 ℃; for 2.5h; Inert atmosphere;

(3-bromoprop-1-yn-1-yl)triethylsilane; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol403709g