2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid potassium salt

Base Information

Chemical Name:2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid potassium salt
CAS No.:1278583-96-2
Molecular Formula:C₂₅H₃₀ClN₂O₇S*K
Molecular Weight:577.14
Hs Code.:

Synonyms:2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid potassium salt

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Chemical Property of 2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid potassium salt

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Technology Process of 2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid potassium salt

There total 7 articles about 2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187857-80-2
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid

: 1278583-96-2
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid potassium salt

Guidance literature:: With potassium hydroxide; In water;

Reference yield:

: 107-35-7
Tau

: 1187856-49-0
2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid

: 1278583-96-2
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid potassium salt

Guidance literature:: Tau; 2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetic acid; With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; water;

With potassium hydroxide; In tetrahydrofuran; water; at 17 ℃; Product distribution / selectivity;

Reference yield:

: 1205-71-6
N-(4-chlorophenyl)aniline

: 1278583-96-2
2-(2-(((1r,4r)-4-(((4-chlorophenyl)(phenyl)carbamoyloxy)methyl)cyclohexyl)methoxy)acetamido)ethanesulfonic acid potassium salt

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium phosphate / acetonitrile / 5.5 h / 65 °C / Inert atmosphere

2.1: acetonitrile / 19 h / 40 - 70 °C / Inert atmosphere

3.1: sodium hydroxide; water; tetrabutylammomium bromide / toluene / 11 h / 20 - 60 °C

3.3: pH 7 - 8

4.1: thionyl chloride / 20 °C

5.1: sodium hydroxide / water; tetrahydrofuran / Cooling with ice

6.1: potassium hydroxide / water

With potassium phosphate; thionyl chloride; tetrabutylammomium bromide; water; potassium hydroxide; sodium hydroxide; In tetrahydrofuran; water; toluene; acetonitrile;