2,3-Dihydrobenzo(C)phenanthren-4(1H)-one

Base Information

• Chemical Name: 2,3-Dihydrobenzo(C)phenanthren-4(1H)-one
• CAS No.: 73093-15-9
• Molecular Formula: C₁₈H₁₄O
• Molecular Weight: 246.309
• NSC Number: 97683
• UNII: 6EE6DZB6XU
• DSSTox Substance ID: DTXSID40223357
• Wikidata: Q83101800

Synonyms:NSC 97683;6EE6DZB6XU;73093-15-9;NSC-97683;2,3-Dihydrobenzo(C)phenanthren-4(1H)-one;11,12-dihydro-10H-benzo[c]phenanthren-9-one;UNII-6EE6DZB6XU;DTXSID40223357;NSC97683;A838550;BENZO(C)PHENANTHREN-4(1H)-ONE, 2,3-DIHYDRO-

Chemical Property of 2,3-Dihydrobenzo(C)phenanthren-4(1H)-one

Chemical Property:

• Vapor Pressure: 1E-08mmHg at 25°C
• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 246.104465066
• Heavy Atom Count: 19
• Complexity: 361

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1CC2=C(C=CC3=C2C4=CC=CC=C4C=C3)C(=O)C1

Technology Process of 2,3-Dihydrobenzo(C)phenanthren-4(1H)-one

There total 4 articles about 2,3-Dihydrobenzo(C)phenanthren-4(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.8%

4-oxo-1,2,3,4,5,6-hexahydrobenzophenanthrene (80285-03-6) → 4-oxo-1,2,3,4-tetrahydrobenzophenanthrene (73093-15-9)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; for 0.333333h; Heating;

DOI:10.1021/jo00340a005

Reference yield:

→ 4-oxo-1,2,3,4-tetrahydrobenzophenanthrene (73093-15-9)

Guidance literature:

With pyridine; thionyl chloride; diethyl ether; Behandeln des erhaltenen Saeurechlorids in Benzol mit SnCl₄ bei Raumtemperatur;

DOI:10.1021/ja01868a023

Reference yield:

pyridine (110-86-1) + thionyl chloride (7719-09-7) + 4-[4]phenanthryl-butyric acid (93875-55-9) + tin(IV) chloride (7646-78-8) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 4-oxo-1,2,3,4-tetrahydrobenzophenanthrene (73093-15-9)

Guidance literature:

DOI:10.1021/ja01868a023

upstream raw materials:

4-oxo-1,2,3,4,5,6-hexahydrobenzophenanthrene

pyridine

thionyl chloride

4-[4]phenanthryl-butyric acid

Downstream raw materials:

3-hydroxybenzophenanthrene

1,2-dihydrobenzophenanthrene

benzo[c]phenathrene

4-methylbenzo[c]phenanthrene

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