3-(4-{[2-({[4-(ethylsulfonyl)phenyl]acetyl}amino)-4-phenyl-1,3-thiazol-5-yl]carbonyl}phenyl)propyl acetate

Base Information

Chemical Name:3-(4-{[2-({[4-(ethylsulfonyl)phenyl]acetyl}amino)-4-phenyl-1,3-thiazol-5-yl]carbonyl}phenyl)propyl acetate
CAS No.:1361414-40-5
Molecular Formula:C₃₁H₃₀N₂O₆S₂
Molecular Weight:590.721
Hs Code.:

Synonyms:3-(4-{[2-({[4-(ethylsulfonyl)phenyl]acetyl}amino)-4-phenyl-1,3-thiazol-5-yl]carbonyl}phenyl)propyl acetate

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Chemical Property of 3-(4-{[2-({[4-(ethylsulfonyl)phenyl]acetyl}amino)-4-phenyl-1,3-thiazol-5-yl]carbonyl}phenyl)propyl acetate

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Technology Process of 3-(4-{[2-({[4-(ethylsulfonyl)phenyl]acetyl}amino)-4-phenyl-1,3-thiazol-5-yl]carbonyl}phenyl)propyl acetate

There total 10 articles about 3-(4-{[2-({[4-(ethylsulfonyl)phenyl]acetyl}amino)-4-phenyl-1,3-thiazol-5-yl]carbonyl}phenyl)propyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 383135-47-5
2-[4-(ethanesulfonyl)phenyl]acetic acid

: 1361414-39-2
3-{4-[(2-amino-4-phenyl-1,3-thiazol-5-yl)carbonyl]phenyl}propyl acetate

: 1361414-40-5
3-(4-{[2-({[4-(ethylsulfonyl)phenyl]acetyl}amino)-4-phenyl-1,3-thiazol-5-yl]carbonyl}phenyl)propyl acetate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; Inert atmosphere;

Reference yield:

: ethyl 2-(4-(ethylthio)phenyl)acetate

: 1361414-40-5
3-(4-{[2-({[4-(ethylsulfonyl)phenyl]acetyl}amino)-4-phenyl-1,3-thiazol-5-yl]carbonyl}phenyl)propyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

2.1: sodium hydroxide; water / ethanol / 20 °C

2.2: pH 1

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 20 °C / Inert atmosphere

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In ethanol; dichloromethane;

Reference yield:

: 122-72-5
3-phenylpropyl acetate

: 1361414-40-5
3-(4-{[2-({[4-(ethylsulfonyl)phenyl]acetyl}amino)-4-phenyl-1,3-thiazol-5-yl]carbonyl}phenyl)propyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum (III) chloride / dichloromethane / 8 h / 0 °C / Inert atmosphere

2: bromine / diethyl ether / 1 h / 0 - 20 °C

3: N,N-dimethyl-formamide / 0.75 h / 85 °C / Inert atmosphere

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 20 °C / Inert atmosphere

With aluminum (III) chloride; bromine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;