7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonylamino]-1,2-dihydrofuro[2,3-c]quinoline-6-carboxylic acid formate salt

Base Information

Chemical Name:7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonylamino]-1,2-dihydrofuro[2,3-c]quinoline-6-carboxylic acid formate salt
CAS No.:1412973-88-6
Molecular Formula:CH₂O₂*C₂₅H₂₆FN₃O₅S
Molecular Weight:545.589
Hs Code.:

Synonyms:7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonylamino]-1,2-dihydrofuro[2,3-c]quinoline-6-carboxylic acid formate salt

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Chemical Property of 7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonylamino]-1,2-dihydrofuro[2,3-c]quinoline-6-carboxylic acid formate salt

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Technology Process of 7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonylamino]-1,2-dihydrofuro[2,3-c]quinoline-6-carboxylic acid formate salt

There total 8 articles about 7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonylamino]-1,2-dihydrofuro[2,3-c]quinoline-6-carboxylic acid formate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-18-6
formic acid

: 1412975-77-9
methyl 7-[N-{2-((Z)-3-diethylaminoprop-1-enyl)-4-fluoro-benzenesulfonyl}-N-(methoxycarbonyl)amino]-1,2-dihydrofuro[2,3-c]quinoline-6-carboxylate

: 1412973-88-6
7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonylamino]-1,2-dihydrofuro[2,3-c]quinoline-6-carboxylic acid formate salt

Guidance literature:: methyl 7-[N-{2-((Z)-3-diethylaminoprop-1-enyl)-4-fluoro-benzenesulfonyl}-N-(methoxycarbonyl)amino]-1,2-dihydrofuro[2,3-c]quinoline-6-carboxylate; With water; lithium hydroxide; In 1,4-dioxane; at 110 ℃; for 2.33333h; Microwave irradiation;

formic acid;

Reference yield:

: 1055881-23-6
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)furan-2-carbaldehyde

: 1412973-88-6
7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonylamino]-1,2-dihydrofuro[2,3-c]quinoline-6-carboxylic acid formate salt

Guidance literature:: Multi-step reaction with 6 steps

1: caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane; water / 1 h / 60 °C / Inert atmosphere

2: 10 wt% Pd(OH)2 on carbon; hydrogen; acetic acid / tetrahydrofuran / 24 h

3: pyridine / dichloromethane / 72 h / 20 °C

4: hydrogen; sodium hydride / tetrahydrofuran / 1 h / 20 °C

5: tri tert-butylphosphoniumtetrafluoroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 1 h / 60 °C / Inert atmosphere

6: lithium hydroxide; water / 1,4-dioxane / 2.33 h / 110 °C / Microwave irradiation

With pyridine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 10 wt% Pd(OH)2 on carbon; water; hydrogen; sodium hydride; caesium carbonate; acetic acid; lithium hydroxide; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;

Reference yield:

: 1356113-88-6
methyl 3-bromo-2,6-diaminobenzoate

: 1412973-88-6
7-[2-((Z)-3-diethylaminoprop-1-enyl)-4-fluorobenzenesulfonylamino]-1,2-dihydrofuro[2,3-c]quinoline-6-carboxylic acid formate salt

Guidance literature:: Multi-step reaction with 6 steps

1: caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane; water / 1 h / 60 °C / Inert atmosphere

2: 10 wt% Pd(OH)2 on carbon; hydrogen; acetic acid / tetrahydrofuran / 24 h

3: pyridine / dichloromethane / 72 h / 20 °C

4: hydrogen; sodium hydride / tetrahydrofuran / 1 h / 20 °C

5: tri tert-butylphosphoniumtetrafluoroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 1 h / 60 °C / Inert atmosphere

6: lithium hydroxide; water / 1,4-dioxane / 2.33 h / 110 °C / Microwave irradiation

With pyridine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 10 wt% Pd(OH)2 on carbon; water; hydrogen; sodium hydride; caesium carbonate; acetic acid; lithium hydroxide; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;