tert-butyl 3-(3-methyl-7-(methylamino)-2-oxo-3,4-dihydropyrimido[4,5-d] pyrimidin-1-(2H)-yl)phenylcarbamate

Base Information

Chemical Name:tert-butyl 3-(3-methyl-7-(methylamino)-2-oxo-3,4-dihydropyrimido[4,5-d] pyrimidin-1-(2H)-yl)phenylcarbamate
CAS No.:1415905-41-7
Molecular Formula:C₁₉H₂₄N₆O₃
Molecular Weight:384.438
Hs Code.:

Synonyms:tert-butyl 3-(3-methyl-7-(methylamino)-2-oxo-3,4-dihydropyrimido[4,5-d] pyrimidin-1-(2H)-yl)phenylcarbamate

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Chemical Property of tert-butyl 3-(3-methyl-7-(methylamino)-2-oxo-3,4-dihydropyrimido[4,5-d] pyrimidin-1-(2H)-yl)phenylcarbamate

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Technology Process of tert-butyl 3-(3-methyl-7-(methylamino)-2-oxo-3,4-dihydropyrimido[4,5-d] pyrimidin-1-(2H)-yl)phenylcarbamate

There total 8 articles about tert-butyl 3-(3-methyl-7-(methylamino)-2-oxo-3,4-dihydropyrimido[4,5-d] pyrimidin-1-(2H)-yl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1363161-19-6
tert-butyl 3-(3-methyl-7-(methylsulfonyl)-2-oxo-3,4-dihydropyrimido[4,5-d]pyrimidin-1(2H)-yl)phenylcarbamate

: 593-51-1
methylamine hydrochloride

: 1415905-41-7
tert-butyl 3-(3-methyl-7-(methylamino)-2-oxo-3,4-dihydropyrimido[4,5-d] pyrimidin-1-(2H)-yl)phenylcarbamate

Guidance literature:: With sodium acetate; In 1,4-dioxane; at 100 ℃; for 24h; Sealed tube;

Reference yield: 89.0%

: 593-51-1
methylamine hydrochloride

: 74-89-5
methylamine

: 1415905-41-7
tert-butyl 3-(3-methyl-7-(methylamino)-2-oxo-3,4-dihydropyrimido[4,5-d] pyrimidin-1-(2H)-yl)phenylcarbamate

Guidance literature:: In 1,4-dioxane;

Reference yield:

: 1363161-18-5
tert-butyl 3-(3-methyl-7-(methylthio)-2-oxo-3,4-dihydropyrimido[4,5-d] pyrimidin-1(2H)-yl) phenylcarbamate

: 1415905-41-7
tert-butyl 3-(3-methyl-7-(methylamino)-2-oxo-3,4-dihydropyrimido[4,5-d] pyrimidin-1-(2H)-yl)phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C

2: sodium acetate / 1,4-dioxane / 24 h / 100 °C / Sealed tube

With sodium acetate; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; dichloromethane;