6-C-prenyl-3,3',4',7-tetra-O-methoxymethylquercetin

Base Information

Chemical Name:6-C-prenyl-3,3',4',7-tetra-O-methoxymethylquercetin
CAS No.:143724-73-6
Molecular Formula:C₂₈H₃₄O₁₁
Molecular Weight:546.571
Hs Code.:

Synonyms:6-C-prenyl-3,3',4',7-tetra-O-methoxymethylquercetin

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Chemical Property of 6-C-prenyl-3,3',4',7-tetra-O-methoxymethylquercetin

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Technology Process of 6-C-prenyl-3,3',4',7-tetra-O-methoxymethylquercetin

There total 4 articles about 6-C-prenyl-3,3',4',7-tetra-O-methoxymethylquercetin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 143724-71-4
5-O-prenyl-3,3',7,4'-tetrakis-O-methoxymethylquercetin

: 143724-73-6
6-C-prenyl-3,3',4',7-tetra-O-methoxymethylquercetin

Guidance literature:: With montmorillonite K₁₀ Clay; In toluene; for 4h; regioselective reaction; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2019.151138

Reference yield:

: 117-39-5,74893-81-5
quercetol

: 143724-73-6
6-C-prenyl-3,3',4',7-tetra-O-methoxymethylquercetin

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / K₂CO₃ / acetone / 2 h / Ambient temperature

2: 2 percent / K₂CO₃ / methanol / 3 h / Ambient temperature

With potassium carbonate; In methanol; acetone;

Reference yield:

: 117-39-5,74893-81-5
quercetol

: 143724-73-6
6-C-prenyl-3,3',4',7-tetra-O-methoxymethylquercetin

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 0.5 h / 20 °C

1.2: 20 °C

2.1: potassium carbonate / acetone / 0.5 h / 20 °C

2.2: 4 h / 45 °C

3.1: montmorillonite K₁₀ Clay / toluene / 4 h / Inert atmosphere; Reflux

With montmorillonite K₁₀ Clay; potassium carbonate; In acetone; toluene;
DOI:10.1016/j.tetlet.2019.151138