4-{[2-(4-nitrophenyl)ethoxycarbonyl]amino}-N¹-(β-D-ribofuranosyl)-1H-imidazo[4,5-c]pyridine

Base Information

• Chemical Name: 4-{[2-(4-nitrophenyl)ethoxycarbonyl]amino}-N¹-(β-D-ribofuranosyl)-1H-imidazo[4,5-c]pyridine
• CAS No.: 738613-48-4
• Molecular Formula: C₂₀H₂₁N₅O₈
• Molecular Weight: 459.415

Synonyms:4-{[2-(4-nitrophenyl)ethoxycarbonyl]amino}-N¹-(β-D-ribofuranosyl)-1H-imidazo[4,5-c]pyridine

Chemical Property of 4-{[2-(4-nitrophenyl)ethoxycarbonyl]amino}-N¹-(β-D-ribofuranosyl)-1H-imidazo[4,5-c]pyridine

Chemical Property:

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Technology Process of 4-{[2-(4-nitrophenyl)ethoxycarbonyl]amino}-N¹-(β-D-ribofuranosyl)-1H-imidazo[4,5-c]pyridine

There total 1 articles about 4-{[2-(4-nitrophenyl)ethoxycarbonyl]amino}-N¹-(β-D-ribofuranosyl)-1H-imidazo[4,5-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

2-(4-nitrophenyl)ethoxycarbonyl chloride (88091-68-3) + 3-deazaadenosine (6736-58-9) → 4-{[2-(4-nitrophenyl)ethoxycarbonyl]amino}-N1-(β-D-ribofuranosyl)-1H-imidazo[4,5-c]pyridine (738613-48-4)

Guidance literature:

3-deazaadenosine; With pyridine; chloro-trimethyl-silane; for 1.5h;

2-(4-nitrophenyl)ethoxycarbonyl chloride;

With ammonia; In water; for 0.5h;

DOI:10.1016/j.bmc.2004.04.021

Reference yield: 73.0%

mono-4-methoxytrityl chloride (14470-28-1) + 4-{[2-(4-nitrophenyl)ethoxycarbonyl]amino}-N1-(β-D-ribofuranosyl)-1H-imidazo[4,5-c]pyridine (738613-48-4) → 4-{[2-(4-nitrophenyl)ethoxycarbonyl]amino}-N1-[5-O-(4-monomethoxytrityl)-β-D-ribofuranosyl]-1H-imidazo[4,5-c]pyridine (738613-49-5)

Guidance literature:

With pyridine; for 24h;

DOI:10.1016/j.bmc.2004.04.021

upstream raw materials:

2-(4-nitrophenyl)ethoxycarbonyl chloride

3-deazaadenosine

Downstream raw materials:

4-{[2-(4-nitrophenyl)ethoxycarbonyl]amino}-N¹-[5-O-(4-monomethoxytrityl)-β-D-ribofuranosyl]-1H-imidazo[4,5-c]pyridine

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