(6S,9S,12S)-methyl 6-(3-iodo-4-methoxyphenyl)-1 2-(4-methoxy-3-(4,4,5 ,5-tetramethyl-1,3 ,2-dioxaborolan-2-yl)benzyl)-2,2,5 ,9-tetramethyl-4,7, 1 0-trioxo-3-oxa-5 ,8,11-triazatridecan-13-oate

Base Information

Chemical Name:(6S,9S,12S)-methyl 6-(3-iodo-4-methoxyphenyl)-1 2-(4-methoxy-3-(4,4,5 ,5-tetramethyl-1,3 ,2-dioxaborolan-2-yl)benzyl)-2,2,5 ,9-tetramethyl-4,7, 1 0-trioxo-3-oxa-5 ,8,11-triazatridecan-13-oate
CAS No.:1086702-98-8
Molecular Formula:C₃₅H₄₉BIN₃O₁₀
Molecular Weight:809.504
Hs Code.:

(6S,9S,12S)-methyl 6-(3-iodo-4-methoxyphenyl)-1 2-(4-methoxy-3-(4,4,5 ,5-tetramethyl-1,3 ,2-dioxaborolan-2-yl)benzyl)-2,2,5 ,9-tetramethyl-4,7, 1 0-trioxo-3-oxa-5 ,8,11-triazatridecan-13-oate

Synonyms:(6S,9S,12S)-methyl 6-(3-iodo-4-methoxyphenyl)-1 2-(4-methoxy-3-(4,4,5 ,5-tetramethyl-1,3 ,2-dioxaborolan-2-yl)benzyl)-2,2,5 ,9-tetramethyl-4,7, 1 0-trioxo-3-oxa-5 ,8,11-triazatridecan-13-oate

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Chemical Property of (6S,9S,12S)-methyl 6-(3-iodo-4-methoxyphenyl)-1 2-(4-methoxy-3-(4,4,5 ,5-tetramethyl-1,3 ,2-dioxaborolan-2-yl)benzyl)-2,2,5 ,9-tetramethyl-4,7, 1 0-trioxo-3-oxa-5 ,8,11-triazatridecan-13-oate

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Technology Process of (6S,9S,12S)-methyl 6-(3-iodo-4-methoxyphenyl)-1 2-(4-methoxy-3-(4,4,5 ,5-tetramethyl-1,3 ,2-dioxaborolan-2-yl)benzyl)-2,2,5 ,9-tetramethyl-4,7, 1 0-trioxo-3-oxa-5 ,8,11-triazatridecan-13-oate

There total 13 articles about (6S,9S,12S)-methyl 6-(3-iodo-4-methoxyphenyl)-1 2-(4-methoxy-3-(4,4,5 ,5-tetramethyl-1,3 ,2-dioxaborolan-2-yl)benzyl)-2,2,5 ,9-tetramethyl-4,7, 1 0-trioxo-3-oxa-5 ,8,11-triazatridecan-13-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1086702-96-6
C₃₄H₄₇BIN₃O₁₀

: 18107-18-1
diazomethyl-trimethyl-silane

: 1086702-98-8
(6S,9S,12S)-methyl 6-(3-iodo-4-methoxyphenyl)-1 2-(4-methoxy-3-(4,4,5 ,5-tetramethyl-1,3 ,2-dioxaborolan-2-yl)benzyl)-2,2,5 ,9-tetramethyl-4,7, 1 0-trioxo-3-oxa-5 ,8,11-triazatridecan-13-oate

Guidance literature:: In methanol; dichloromethane; at 20 ℃;
DOI:10.1055/s-2008-1078209

Reference yield:

: 1004524-42-8
(S)-methyl 2-amino-3-(4-methoxy-3-(4,4,5 ,5-tetramethyl-1,3 ,2-dioxaborolan-2-yl)phenyl)propanoate

: 1253795-20-8
(S)-3-((S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(3-iodo-4-methoxyphenyl)acetamido)-2-oxobutanoic acid

: 1086702-98-8
(6S,9S,12S)-methyl 6-(3-iodo-4-methoxyphenyl)-1 2-(4-methoxy-3-(4,4,5 ,5-tetramethyl-1,3 ,2-dioxaborolan-2-yl)benzyl)-2,2,5 ,9-tetramethyl-4,7, 1 0-trioxo-3-oxa-5 ,8,11-triazatridecan-13-oate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃;

Reference yield:

: 94790-24-6
(S)-methyl 2-((tert-butoxycarbonyl)amino)-3-(4-methoxyphenyl)propanoate

: 1086702-98-8
(6S,9S,12S)-methyl 6-(3-iodo-4-methoxyphenyl)-1 2-(4-methoxy-3-(4,4,5 ,5-tetramethyl-1,3 ,2-dioxaborolan-2-yl)benzyl)-2,2,5 ,9-tetramethyl-4,7, 1 0-trioxo-3-oxa-5 ,8,11-triazatridecan-13-oate

Guidance literature:: Multi-step reaction with 4 steps

1: silver sulfate; iodine / methanol / 2 h / 20 °C

2: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 3 h / 80 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 20 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide; acetonitrile / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; iodine; potassium acetate; benzotriazol-1-ol; silver sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;