C₄₆H₄₄ClN₃O₇S

Base Information

Chemical Name:C₄₆H₄₄ClN₃O₇S
CAS No.:1352714-17-0
Molecular Formula:C₄₆H₄₄ClN₃O₇S
Molecular Weight:818.39
Hs Code.:

C<sub>46</sub>H<sub>44</sub>ClN<sub>3</sub>O<sub>7</sub>S

Synonyms:C₄₆H₄₄ClN₃O₇S

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Chemical Property of C₄₆H₄₄ClN₃O₇S

Chemical Property:

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Technology Process of C₄₆H₄₄ClN₃O₇S

There total 8 articles about C₄₆H₄₄ClN₃O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1260242-00-9
(2R,3R,4R,5S)-3,4,5-tris(benzyloxy)-2-(benzyloxymethyl)-6-(3-(bromomethyl)-4-chlorophenyl)-tetrahydro-2H-pyran

: 1352714-17-0
C₄₆H₄₄ClN₃O₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: ethanol; water / 15 h / Reflux

2.1: sodium hydroxide; water / ethanol / Reflux

2.2: 20 °C

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 5.25 h / 0 - 20 °C / Inert atmosphere

4.1: ammonium hydroxide / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere

5.1: Lawessons reagent / tetrahydrofuran / 15 h / Reflux; Inert atmosphere

6.1: pyridine / ethanol / 15 h / 80 °C / Inert atmosphere

7.1: potassium hydroxide; ethanol / tetrahydrofuran / 2 h / Reflux; Inert atmosphere

8.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 4-methyl-morpholine / N,N-dimethyl-formamide / 15 h / 20 °C / Inert atmosphere

With Lawessons reagent; 4-methyl-morpholine; pyridine; ammonium hydroxide; oxalyl dichloride; ethanol; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1225430-37-4
(2-chloro-5-((3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)phenyl)methanol

: 1352714-17-0
C₄₆H₄₄ClN₃O₇S

Guidance literature:: Multi-step reaction with 9 steps

1.1: pyridine; phosphorus tribromide / diethyl ether / 16 h / 0 °C / Reflux; Inert atmosphere

2.1: ethanol; water / 15 h / Reflux

3.1: sodium hydroxide; water / ethanol / Reflux

3.2: 20 °C

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 5.25 h / 0 - 20 °C / Inert atmosphere

5.1: ammonium hydroxide / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere

6.1: Lawessons reagent / tetrahydrofuran / 15 h / Reflux; Inert atmosphere

7.1: pyridine / ethanol / 15 h / 80 °C / Inert atmosphere

8.1: potassium hydroxide; ethanol / tetrahydrofuran / 2 h / Reflux; Inert atmosphere

9.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 4-methyl-morpholine / N,N-dimethyl-formamide / 15 h / 20 °C / Inert atmosphere

With Lawessons reagent; 4-methyl-morpholine; pyridine; ammonium hydroxide; oxalyl dichloride; ethanol; water; phosphorus tribromide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1225430-39-6
2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)phenyl)acetonitrile

: 1352714-17-0
C₄₆H₄₄ClN₃O₇S

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydroxide; water / ethanol / Reflux

1.2: 20 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 5.25 h / 0 - 20 °C / Inert atmosphere

3.1: ammonium hydroxide / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere

4.1: Lawessons reagent / tetrahydrofuran / 15 h / Reflux; Inert atmosphere

5.1: pyridine / ethanol / 15 h / 80 °C / Inert atmosphere

6.1: potassium hydroxide; ethanol / tetrahydrofuran / 2 h / Reflux; Inert atmosphere

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 4-methyl-morpholine / N,N-dimethyl-formamide / 15 h / 20 °C / Inert atmosphere

With Lawessons reagent; 4-methyl-morpholine; pyridine; ammonium hydroxide; oxalyl dichloride; ethanol; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;