methyl 4-(L-isoleucinylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride

Base Information

Chemical Name:methyl 4-(L-isoleucinylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride
CAS No.:1038451-60-3
Molecular Formula:C₁₉H₂₅N₃O₃*ClH
Molecular Weight:379.887
Hs Code.:

Synonyms:methyl 4-(L-isoleucinylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride

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Chemical Property of methyl 4-(L-isoleucinylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride

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Technology Process of methyl 4-(L-isoleucinylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride

There total 1 articles about methyl 4-(L-isoleucinylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1038451-54-5
methyl 4-[N-(9-fluorenylmethoxycarbonyl)-L-isoleucinylbenzylamino]-1H-pyrrole-2-carboxylate

: 1038451-60-3
methyl 4-(L-isoleucinylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride

Guidance literature:: methyl 4-[N-(9-fluorenylmethoxycarbonyl)-L-isoleucinylbenzylamino]-1H-pyrrole-2-carboxylate; With piperidine; In N,N-dimethyl-formamide; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; Inert atmosphere;
DOI:10.1021/ol8009978

Reference yield: 72.0%

: 1038451-60-3
methyl 4-(L-isoleucinylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride

: 100-52-7
benzaldehyde

: 1038451-74-9
(3S,5R)-methyl 1-benzyl-3-[(1S)-1-methylpropyl]-5-phenyl-3H,5H-pyrrolo[3,2-e][1,4]diazepin-2-one-7-carboxylate

Guidance literature:: methyl 4-(L-isoleucinylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride; benzaldehyde; With trifluoroacetic acid; In toluene; at 70 ℃; for 48h; Molecular sieve; Inert atmosphere; Sealed tube;

With sodium hydroxide; In water; toluene; at 20 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol8009978

Reference yield: 64.0%

: 1038451-60-3
methyl 4-(L-isoleucinylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride

: 78-84-2
isobutyraldehyde

: 1038451-91-0
(3S,5R)-methyl 1-benzyl-3-[(1S)-1-methylpropyl]-5-isopropyl-3H,5H-pyrrolo[3,2-e][1,4]diazepin-2-one-7-carboxylate

Guidance literature:: methyl 4-(L-isoleucinylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride; isobutyraldehyde; With trifluoroacetic acid; In toluene; at 70 ℃; for 48h; Molecular sieve; Inert atmosphere; Sealed tube;

With sodium hydroxide; In water; toluene; at 20 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol8009978