Pyridine, 1-acetyl-1,2,3,4-tetrahydro-6-(nitromethyl)- (9CI)

Base Information

Chemical Name:Pyridine, 1-acetyl-1,2,3,4-tetrahydro-6-(nitromethyl)- (9CI)
CAS No.:176042-68-5
Molecular Formula:C₈H₁₂N₂O₃
Molecular Weight:184.195
Hs Code.:
Mol file:176042-68-5.mol

Synonyms:Pyridine,1-acetyl-1,2,3,4-tetrahydro-6-(nitromethyl)- (9CI)

Suppliers and Price of Pyridine, 1-acetyl-1,2,3,4-tetrahydro-6-(nitromethyl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pyridine, 1-acetyl-1,2,3,4-tetrahydro-6-(nitromethyl)- (9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Pyridine, 1-acetyl-1,2,3,4-tetrahydro-6-(nitromethyl)- (9CI)

There total 3 articles about Pyridine, 1-acetyl-1,2,3,4-tetrahydro-6-(nitromethyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

: 75-36-5
acetyl chloride

: 57023-05-9
SD 33420

: 1'-acetyl-2-(nitromethylene)-piperidine

: 176042-68-5
1-acetyl-2-(nitromethyl)-1,4,5,6-tetrahydropyridine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 25 ℃; for 2h;
DOI:10.1016/S0040-4020(96)00074-9

Reference yield:

: 5693-62-9
2,3,4,5-tetrahydro-6-methoxypyridine

: 176042-68-5
1-acetyl-2-(nitromethyl)-1,4,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / 72 h / Heating

2: 4 percent / diisopropylethylamine / CH₂Cl₂ / 2 h / 25 °C

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4020(96)00074-9

Reference yield:

: 675-20-7
piperidin-2-one

: 176042-68-5
1-acetyl-2-(nitromethyl)-1,4,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 39 percent / benzene / 16 h / Heating

2: 49 percent / 72 h / Heating

3: 4 percent / diisopropylethylamine / CH₂Cl₂ / 2 h / 25 °C

With N-ethyl-N,N-diisopropylamine; In dichloromethane; benzene;
DOI:10.1016/S0040-4020(96)00074-9