9-[2,3-dideoxy-2-fluoro-5-O-(triphenylmethyl)-β-D-threo-pentofuranosyl]-9H-purine-6-amine

Base Information

Chemical Name:9-[2,3-dideoxy-2-fluoro-5-O-(triphenylmethyl)-β-D-threo-pentofuranosyl]-9H-purine-6-amine
CAS No.:234436-55-6
Molecular Formula:C₂₉H₂₆FN₅O₂
Molecular Weight:495.556
Hs Code.:

Synonyms:9-[2,3-dideoxy-2-fluoro-5-O-(triphenylmethyl)-β-D-threo-pentofuranosyl]-9H-purine-6-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-[2,3-dideoxy-2-fluoro-5-O-(triphenylmethyl)-β-D-threo-pentofuranosyl]-9H-purine-6-amine

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 9-[2,3-dideoxy-2-fluoro-5-O-(triphenylmethyl)-β-D-threo-pentofuranosyl]-9H-purine-6-amine

There total 27 articles about 9-[2,3-dideoxy-2-fluoro-5-O-(triphenylmethyl)-β-D-threo-pentofuranosyl]-9H-purine-6-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 244140-87-2
6-chloro-9-[2,3-dideoxy-2-fluoro-5-O-(triphenylmethyl)-β-D-threo-pentofuranosyl]-9H-purine

: 234436-55-6
9-[2,3-dideoxy-2-fluoro-5-O-(triphenylmethyl)-β-D-threo-pentofuranosyl]-9H-purine-6-amine

Guidance literature:: With ammonia; In tetrahydrofuran; at 70 ℃; for 72h; under 5250.42 - 6000.48 Torr;
DOI:10.1081/NCN-120016572

Reference yield: 93.0%

: 265987-43-7
9-(5-O-trityl-3-O-methylthiothiocarbonyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl) adenine

: 234436-55-6
9-[2,3-dideoxy-2-fluoro-5-O-(triphenylmethyl)-β-D-threo-pentofuranosyl]-9H-purine-6-amine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); hypophosphorous acid; triethylamine; In 1,2-dimethoxyethane; for 1.8h; Heating;
DOI:10.1016/S0040-4039(01)01617-3

Reference yield: 81.0%

: 234436-54-5
9-(3-O-phenoxythiocarbonyl-5-O-trityl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)adenine

: 234436-55-6
9-[2,3-dideoxy-2-fluoro-5-O-(triphenylmethyl)-β-D-threo-pentofuranosyl]-9H-purine-6-amine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); diphenylsilane; In 1,4-dioxane; Further Variations:; Reagents; Solvents; Product distribution;
DOI:10.1016/S0040-4039(01)00135-6