Cy₂AsCH₂PCy₂

Base Information

Chemical Name:Cy₂AsCH₂PCy₂
CAS No.:206752-72-9
Molecular Formula:C₂₅H₄₆AsP
Molecular Weight:452.536
Hs Code.:

Cy<sub>2</sub>AsCH<sub>2</sub>PCy<sub>2</sub>

Synonyms:Cy₂AsCH₂PCy₂

Suppliers and Price of Cy₂AsCH₂PCy₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cy₂AsCH₂PCy₂

Chemical Property:

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Technology Process of Cy₂AsCH₂PCy₂

There total 1 articles about Cy₂AsCH₂PCy₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 3617-38-7
Chlordicyclohexylarsan

: Cy₂PCH₂SnPh₃

: 206752-72-9
Cy₂AsCH₂PCy₂

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; phenyllithium; In diethyl ether; cyclohexane; at -78 - 20 ℃;

Reference yield: 83.0%

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 206752-72-9
Cy₂AsCH₂PCy₂

: 206752-47-8
(η(4)-cyclooctadiene)RhCl(κ-P-Cy2PCH2AsCy2)

Guidance literature:: In hexane; pentane; Ar-atmosphere; stirring for 10 min at room temp.; evapn., washing (Me2CO), drying; elem. anal.;
DOI:10.1021/om971085o

Reference yield: 74.0%

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 26042-63-7
silver(I) hexafluorophosphate

: 206752-72-9
Cy₂AsCH₂PCy₂

: 206752-54-7
[(η(4)-cyclooctadiene)Rh(κ(2)-As,P-Cy2AsCH2PCy2)]PF6

Guidance literature:: In dichloromethane; byproducts: AgCl; Ar-atmosphere; stirring soln. of Rh-complex and P/As-ligand for 10 min at room temp., addn. of soln. of AgPF6, stirring for 1 h under exclusion of light; filtration off of AgCl, evapn., crystn. (MeOH, -60°C), collection, washing (pentane), drying; elem. anal.;
DOI:10.1021/om971085o