4-(1-bromo-1,1,2,3,3,3-hexafluoropropan-2-yl)-6-(difluoromethoxy)aniline

Base Information

Chemical Name:4-(1-bromo-1,1,2,3,3,3-hexafluoropropan-2-yl)-6-(difluoromethoxy)aniline
CAS No.:1262665-43-9
Molecular Formula:C₁₀H₆BrF₈NO
Molecular Weight:388.055
Hs Code.:

Synonyms:4-(1-bromo-1,1,2,3,3,3-hexafluoropropan-2-yl)-6-(difluoromethoxy)aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(1-bromo-1,1,2,3,3,3-hexafluoropropan-2-yl)-6-(difluoromethoxy)aniline

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Technology Process of 4-(1-bromo-1,1,2,3,3,3-hexafluoropropan-2-yl)-6-(difluoromethoxy)aniline

There total 1 articles about 4-(1-bromo-1,1,2,3,3,3-hexafluoropropan-2-yl)-6-(difluoromethoxy)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 661-95-0
1,2-dibromohexafluoropropane

: 22236-04-0
2-(difluoromethoxy)aniline

: 1262665-43-9
4-(1-bromo-1,1,2,3,3,3-hexafluoropropan-2-yl)-6-(difluoromethoxy)aniline

Guidance literature:: With sodium dithionite; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; In tert-butyl methyl ether; water; at 18 - 30 ℃; for 48h;

Reference yield: 75.0%

: 1262665-43-9
4-(1-bromo-1,1,2,3,3,3-hexafluoropropan-2-yl)-6-(difluoromethoxy)aniline

: 1262665-44-0
2-bromo-4-(1-bromo-1,1,2,3,3,3-hexafluoropropan-2-yl)-6-(difluoromethoxy)aniline

Guidance literature:: With N-Bromosuccinimide; In acetic acid; at 70 ℃; for 3h;

Reference yield:

: 1262665-43-9
4-(1-bromo-1,1,2,3,3,3-hexafluoropropan-2-yl)-6-(difluoromethoxy)aniline

: 1262663-66-0
N-[2-bromo-4-(1-bromo-1,1,2,3,3,3-hexafluoropropan-2-yl)-6-(difluoromethoxy)phenyl]-2-cyanoquinoline-6-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide / acetic acid / 3 h / 70 °C

2.1: pyridine / dichloromethane / 5 h / Reflux

2.2: 2 h / 18 - 30 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / 18 - 30 °C

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 5 h / 60 °C

With pyridine; N-Bromosuccinimide; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; acetic acid;