methyl (5S,3Z)-5-[N-(tert-butoxycarbonyl)amino]-6-phenyl-4-(trifluoromethyl)hex-3-enoate

Base Information

• Chemical Name: methyl (5S,3Z)-5-[N-(tert-butoxycarbonyl)amino]-6-phenyl-4-(trifluoromethyl)hex-3-enoate
• CAS No.: 1025723-07-2
• Molecular Formula: C₁₉H₂₄F₃NO₄
• Molecular Weight: 387.399

Synonyms:methyl (5S,3Z)-5-[N-(tert-butoxycarbonyl)amino]-6-phenyl-4-(trifluoromethyl)hex-3-enoate

Chemical Property of methyl (5S,3Z)-5-[N-(tert-butoxycarbonyl)amino]-6-phenyl-4-(trifluoromethyl)hex-3-enoate

Chemical Property:

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Technology Process of methyl (5S,3Z)-5-[N-(tert-butoxycarbonyl)amino]-6-phenyl-4-(trifluoromethyl)hex-3-enoate

There total 1 articles about methyl (5S,3Z)-5-[N-(tert-butoxycarbonyl)amino]-6-phenyl-4-(trifluoromethyl)hex-3-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

methanol (67-56-1) + (4S,2Z)-4-[N-(tert-butoxycarbonyl)amino]-5-phenyl-3-(trifluoromethyl)pent-2-enyl methyl carbonate (1025722-70-6) + carbon monoxide (201230-82-2) → methyl (5S,3E)-5-[N-(tert-butoxycarbonyl)amino]-6-phenyl-4-(trifluoromethyl)hex-3-enoate (1025723-08-3) + methyl (5S,3Z)-5-[N-(tert-butoxycarbonyl)amino]-6-phenyl-4-(trifluoromethyl)hex-3-enoate (1025723-07-2)

Guidance literature:

With triphenylphosphine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; at 50 ℃; for 12h; under 22502.3 Torr;

DOI:10.1021/jo702318d

Reference yield: 85.0%

methyl (5S,3Z)-5-[N-(tert-butoxycarbonyl)amino]-6-phenyl-4-(trifluoromethyl)hex-3-enoate (1025723-07-2) → (5S,3Z)-5-amino-6-phenyl-4-(trifluoromethyl)hex-3-enoic acid hydrochloric acid salt

Guidance literature:

With hydrogenchloride; acetic acid; at 100 ℃; for 0.333333h;

DOI:10.1021/jo702318d

upstream raw materials:

methanol

(4S,2Z)-4-[N-(tert-butoxycarbonyl)amino]-5-phenyl-3-(trifluoromethyl)pent-2-enyl methyl carbonate

carbon monoxide

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