1-(1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-ylidene)-2-phenylhydrazine

Base Information

Chemical Name:1-(1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-ylidene)-2-phenylhydrazine
CAS No.:1616560-23-6
Molecular Formula:C₂₁H₂₆N₂O
Molecular Weight:322.45
Hs Code.:

Synonyms:1-(1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-ylidene)-2-phenylhydrazine

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Chemical Property of 1-(1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-ylidene)-2-phenylhydrazine

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Technology Process of 1-(1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-ylidene)-2-phenylhydrazine

There total 2 articles about 1-(1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-ylidene)-2-phenylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1616560-09-8
1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-one

: 100-63-0
phenylhydrazine

: 1616560-22-5
1-(1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-ylidene)-2-phenylhydrazine

: 1616560-23-6
1-(1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-ylidene)-2-phenylhydrazine

Guidance literature:: With acetic acid; In ethanol; at 60 ℃; Inert atmosphere;
DOI:10.1039/c4ob00839a

Reference yield:

: 32097-05-5
4-methoxy-β,β-dimethylacrylophenone

: 1616560-22-5
1-(1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-ylidene)-2-phenylhydrazine

: 1616560-23-6
1-(1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-ylidene)-2-phenylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium tetrachloride / dichloromethane / -78 °C

1.2: 0.58 h / 20 °C

2.1: acetic acid / ethanol / 60 °C / Inert atmosphere

With titanium tetrachloride; acetic acid; In ethanol; dichloromethane;
DOI:10.1039/c4ob00839a