C₁₄H₁₀ClFN₂O

Base Information

Chemical Name:C₁₄H₁₀ClFN₂O
CAS No.:1093097-90-5
Molecular Formula:C₁₄H₁₀ClFN₂O
Molecular Weight:276.698
Hs Code.:

C<sub>14</sub>H<sub>10</sub>ClFN<sub>2</sub>O

Synonyms:C₁₄H₁₀ClFN₂O

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Chemical Property of C₁₄H₁₀ClFN₂O

Chemical Property:

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Technology Process of C₁₄H₁₀ClFN₂O

There total 4 articles about C₁₄H₁₀ClFN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1093097-89-2
C₁₄H₈ClFN₂O₃

: 1093097-90-5
C₁₄H₁₀ClFN₂O

Guidance literature:: With iron; ammonium chloride; In tetrahydrofuran; methanol; water; at 70 ℃; for 1h;

Reference yield:

: 1093097-88-1
C₁₄H₉Cl₂FN₂O₃

: 1093097-90-5
C₁₄H₁₀ClFN₂O

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / N,N-dimethyl-formamide / 1 h / 20 °C

2: iron; ammonium chloride / tetrahydrofuran; methanol; water / 1 h / 70 °C

With sodium hydroxide; iron; ammonium chloride; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 7494-45-3
1,2-dichloro-4-methyl-5-nitrobenzene

: 1093097-90-5
C₁₄H₁₀ClFN₂O

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 2 h / 0 - 20 °C

1.3: 0 °C

2.1: pyridine; hydroxylamine hydrochloride / ethanol / 72 h / 60 °C

3.1: sodium hydroxide / N,N-dimethyl-formamide / 1 h / 20 °C

4.1: iron; ammonium chloride / tetrahydrofuran; methanol; water / 1 h / 70 °C

With pyridine; sodium hydroxide; hydroxylamine hydrochloride; potassium tert-butylate; iron; ammonium chloride; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;