Technology Process of 1-(3-dodecylphenyl)-1-hydroxy-1,2-dihydropyrrolo[3,4-c]pyridine-3-one
There total 6 articles about 1-(3-dodecylphenyl)-1-hydroxy-1,2-dihydropyrrolo[3,4-c]pyridine-3-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; silver(l) oxide;
In
tetrahydrofuran;
at 80 ℃;
for 48h;
Inert atmosphere;
DOI:10.1016/j.ejmech.2010.07.016
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ethanol; sodium tetrahydroborate / 3 h / 20 °C
2.1: formic acid / 24 h / Reflux
2.2: 3 h / 20 °C
2.3: pH 1
3.1: thionyl chloride / 2 h / 60 °C / Inert atmosphere
3.2: 1 h / 20 °C
4.1: potassium carbonate; silver(l) oxide / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 48 h / 80 °C / Inert atmosphere; Sealed tube
4.2: 2 h
With
sodium tetrahydroborate; formic acid; thionyl chloride; ethanol; potassium carbonate; silver(l) oxide;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: formic acid / 24 h / Reflux
1.2: 3 h / 20 °C
1.3: pH 1
2.1: thionyl chloride / 2 h / 60 °C / Inert atmosphere
2.2: 1 h / 20 °C
3.1: potassium carbonate; silver(l) oxide / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 48 h / 80 °C / Inert atmosphere; Sealed tube
3.2: 2 h
With
formic acid; thionyl chloride; potassium carbonate; silver(l) oxide;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran;