3-Bromo-N-methoxy-N-methylbenzamide

Base Information

Chemical Name:3-Bromo-N-methoxy-N-methylbenzamide
CAS No.:207681-67-2
Molecular Formula:C9H10 Br N O2
Molecular Weight:244.088
Hs Code.:2924299090
European Community (EC) Number:958-457-5
DSSTox Substance ID:DTXSID90478936
Nikkaji Number:J1.581.518C
Wikidata:Q82312672
Mol file:207681-67-2.mol

Synonyms:3-Bromo-N-methoxy-N-methylbenzamide;207681-67-2;Benzamide, 3-bromo-N-methoxy-N-methyl-;MFCD02684302;SCHEMBL935497;DTXSID90478936;VPWARUVASBJSPY-UHFFFAOYSA-N;AB8379;AKOS008917341;AC-16334;AS-76850;SY142844;CS-0186795;FT-0651133;EN300-105112;F1903-0132

Suppliers and Price of 3-Bromo-N-methoxy-N-methylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3-Bromo-N-methoxy-N-methylbenzamide 95+%
10g
$ 299.00

American Custom Chemicals Corporation
3-BROMO-N-METHOXY-N-METHYLBENZAMIDE 95.00%
5G
$ 1590.46

American Custom Chemicals Corporation
3-BROMO-N-METHOXY-N-METHYLBENZAMIDE 95.00%
2.5G
$ 1255.54

American Custom Chemicals Corporation
3-BROMO-N-METHOXY-N-METHYLBENZAMIDE 95.00%
1G
$ 867.10

Alichem
3-Bromo-N-methoxy-N-methylbenzamide
10g
$ 244.00

Alichem
3-Bromo-N-methoxy-N-methylbenzamide
5g
$ 156.56

Activate Scientific
3-Bromo-N-methoxy-N-methylbenzamide 98%
5 g
$ 309.00

Total 11 raw suppliers

Chemical Property of 3-Bromo-N-methoxy-N-methylbenzamide

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Refractive Index:1.56
Boiling Point:352.95°C at 760 mmHg
Flash Point:167.258°C
PSA：29.54000
Density:1.459g/cm³
LogP:2.08250
Storage Temp.:2-8°C
XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:242.98949
Heavy Atom Count:13
Complexity:187

Purity/Quality:

97% ^*data from raw suppliers

3-Bromo-N-methoxy-N-methylbenzamide 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C(=O)C1=CC(=CC=C1)Br)OC

Technology Process of 3-Bromo-N-methoxy-N-methylbenzamide

There total 9 articles about 3-Bromo-N-methoxy-N-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 585-76-2
m-bromobenzoic acid

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 207681-67-2
N-methoxy-N-methyl-3-bromobenzamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In water; acetonitrile; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.ejmech.2010.07.016

Reference yield: 94.0%

: 591-18-4
1-Bromo-3-iodobenzene

: 201230-82-2
carbon monoxide

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 207681-67-2
N-methoxy-N-methyl-3-bromobenzamide

Guidance literature:: With potassium carbonate; In toluene; at 105 ℃; for 12h; under 2250.23 Torr; Inert atmosphere; Green chemistry;
DOI:10.1039/c4ra04614e

Reference yield: 89.3%

: 585-76-2
m-bromobenzoic acid

: Ν,Ο-dimethylhydroxylamine hydrochloride

: 207681-67-2
N-methoxy-N-methyl-3-bromobenzamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 24h;