1-(3-dodecylphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium

Base Information

Chemical Name:1-(3-dodecylphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium
CAS No.:1180022-76-7
Molecular Formula:C₂₉H₄₁N₂O₄
Molecular Weight:481.656
Hs Code.:

Synonyms:1-(3-dodecylphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium

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Chemical Property of 1-(3-dodecylphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium

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Technology Process of 1-(3-dodecylphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium

There total 6 articles about 1-(3-dodecylphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1179810-87-7
1-(3-dodecylphenyl)-1-hydroxy-1,2-dihydropyrrolo[3,4-c]pyridine-3-one

: 105-36-2
ethyl bromoacetate

: 1180022-76-7
1-(3-dodecylphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium

Guidance literature:: In tetrahydrofuran; for 48h; Reflux; Inert atmosphere;

Reference yield:

: 207681-67-2
N-methoxy-N-methyl-3-bromobenzamide

: 1180022-76-7
1-(3-dodecylphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium diisopropyl amide / n-heptane; diethyl ether; tetrahydrofuran / -78 - -50 °C / Inert atmosphere

1.2: -78 - 20 °C

2.1: ethanol; sodium tetrahydroborate / 3 h / 20 °C

3.1: formic acid / 24 h / Reflux

3.2: 3 h / 20 °C

3.3: pH 1

4.1: thionyl chloride / 2 h / 60 °C / Inert atmosphere

4.2: 1 h / 20 °C

5.1: potassium carbonate; silver(l) oxide / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 48 h / 80 °C / Inert atmosphere; Sealed tube

5.2: 2 h

6.1: tetrahydrofuran / 48 h / Reflux; Inert atmosphere

With sodium tetrahydroborate; formic acid; thionyl chloride; ethanol; potassium carbonate; silver(l) oxide; lithium diisopropyl amide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; diethyl ether; n-heptane;

Reference yield:

: 1179811-02-9
4-(3-bromobenzoyl)-N,N-diisopropylnicotinamide

: 1180022-76-7
1-(3-dodecylphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethanol; sodium tetrahydroborate / 3 h / 20 °C

2.1: formic acid / 24 h / Reflux

2.2: 3 h / 20 °C

2.3: pH 1

3.1: thionyl chloride / 2 h / 60 °C / Inert atmosphere

3.2: 1 h / 20 °C

4.1: potassium carbonate; silver(l) oxide / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 48 h / 80 °C / Inert atmosphere; Sealed tube

4.2: 2 h

5.1: tetrahydrofuran / 48 h / Reflux; Inert atmosphere

With sodium tetrahydroborate; formic acid; thionyl chloride; ethanol; potassium carbonate; silver(l) oxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran;